摘要
Anoveltwo-stagereductionprocessforsynthesisofultrafinenickelpowderwithahighpurityandlowdensityinafluidizedbedreactorhasbeendevelopedinthiswork.TherawultrafineNiOparticlesarefirstpre-reducedusinghydrogenatlowertemperatures(340-400℃),followedbyfurtherreductionathighertemperatures(500-600℃).Theself-agglomerationofNiparticlesformedduringlow-temperaturereductiondecreasesthesinteringactivityofthenewlyformedultrafineNiparticles,leadingtogoodfluidizationquality,evenforthesubsequenthigh-temperaturereductionprocess.TheagglomeratedNiparticleshaveahighNicontent(above99wt%),alowdensity(0.78g/cm~3)andauniformparticlesize(approximately100μm).Aconceptdesignforanoveltwo-stagefluidizedbedreactorprocessusedtoproducehigh-purityNipowderwasalsoproposed.Thisapproachmaybeextendedtothesynthesisofotherultrafine/nanosizedmetalsormetaloxidesthroughafluidizationmethod.
出版日期
2015年02月12日（中国期刊网平台首次上网日期，不代表论文的发表时间）
