An Absolute Method for Determination of Thermal Conductivities of Thermal Insulators by Microcalorimetry-中国期刊网

摘要 Microcalorimetrywasdevelopedtodeterminethermalconductivities(λ)ofthermalinsulatorswithhollowcylindricalshapes,Aspecialdeviceofspecimentwithresistancethreadswrappedonitssurfaceandelectricheaterplacedinitsholewasdesignedtomeettheneedsofdeterminingλwithoutusingstandardsubstancestocalibratetheinstrument.Aformulaforcalculatingthevalueofλwasderived.Byheatingintheholeandonthesurfaceofthespecimenrespectively,thevaluesofλcanbeobtainedconvenientlybythistechnique.Themethodwastestedwithteflon,plexiglass,quartzglassandp[olyethylene.Theexperimentalvaluesofλforthefoursubstancesagreewellwiththeliteraturesones.Erroranalysiswasalsomadeontheexperimentaldata.Itwasfounrthatthemainfactorsaffectingvaluesofλare:(1)Theerroreofdeterminingthevaluesofheatcumulatedinspecimenandmaterialsinthespacearounditand(2)theerroreofdeterminingthevaluesofinnerandouterradiiofcylindricalspecimen.λ

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An Absolute Method for Determination of Thermal Conductivities of Thermal Insulators by Microcalorimetry

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An Absolute Method for Determination of Thermal Conductivities of Thermal Insulators by Microcalorimetry

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