NEW FLUOROSILOXANE AS A COATING MATERIAL FOR NERVE AGENT SENSORS-中国期刊网

摘要 Polymercoatedquartzcrystalmicrobalance(QCM)sensorbasedonthefrequencyshiftsduetotheadsorptionofcompoundsatthesurfaceofmodifiedquartzcrystalelectrodeisaneffectivemethodfordetectionofsarin(GB)whichisahighlytoxicnervewarfareagent.Anewfluorosiloxanepolymerhasbeensynthesizedthrough6stepsfromtrifluoromethylbenzene.Thesynthesiswasachievedfromtrifluoromethylbenzenethroughnitration,hydrogenation.Theobtainedm-nitrotrifluoromethylanilinewastreatedwithNaNO2,andthenhydrolyzedtom-nitrotrifluoromethylphenol.m-nitrotrifluoromethylphenolwasreactedwithallylbromidetotheetherproduct.TheproductwasrearrangedbyClaisenrearrangement,andthenreactedwithpolymethylhydrosiloxaneundercatalystofPt/DVTMS.Thefluorosiloxanepolymercanbeobtained.ThepolymerhasbeensuccessfullyusedasQCMcoatingmaterial.

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NEW FLUOROSILOXANE AS A COATING MATERIAL FOR NERVE AGENT SENSORS

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NEW FLUOROSILOXANE AS A COATING MATERIAL FOR NERVE AGENT SENSORS

来源期刊

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