简介:PureAl2O3-2SiO2powderswerepreparedbysol-gelandcoprecipitationmethods,andtheiralkaliactivationreactivitieswerecompared.Thealkali-activationreactivityofthepowderpreparedbythesol-gelmethodwashigherthanthatofthepowderpreparedbythecoprecipitationmethod.Thepowderswereinvestigatedby27AIand29Simagic-anglespinningnuclearmagneticresonancespectroscopy(MASNMR)tounderstandtherelationshipbetweentheirstructureandalkali-activationreactivity.The27AlMASNMRdatashowedthatthefive-coordinateAIcontentofthepowderpreparedbythesol-gelmethodwashigherthanthatofthepowderpreparedbycoprecipitation.Thehighercontentoffive-coordinateAlcorrespondedtohigheralkali-activationreactivity.The29SiMASNMRdatashowedthatforthepowderpreparedbythesol-gelmethod,siliconwasreplacedbyaluminumatsecondarycoordinationsitesofthecentralSiatomsduringcalcination.However,forthepowderpreparedbysingle-batchcoprecipitation,themainchangewasfromalowdegreeofpolycondensationtoahighdegreeofpolycondensation.
简介:Lithium-aluminum-cobalt-nickeloxideLiAlxCoyNi1xyO2particles,generallyusedascathodeoflithiumbattery,werepreparedbychemicalcoprecipitationfromanaqueoussolutionofLiOH,Al(NO3)3,Co(NO3)2andNi(NO3)2withNH4OH.XRD,SEMandFTIRwereusedtoexaminetheeffectofnickelcontentontheproduct.FTIRpatternsshowedthatincreaseinnickelcontentdecreasedtheabsorptionstrengthofthepeakofspinelstructureoftheproduct,attributedtotheoccupationbynickelinthealuminumsites.Particlesizeandelectricalpropertiesofthelithium-aluminum-cobalt-nickeloxide(abbreviatedasLACNO)particleswerealsodetermined.
简介:The(2+1)-dimensionalBKPequationintheHirotabilinearformisstudiedduringthiswork.WronskianandGrammiantechniquesareappliedtotheconstructionofWronskianandGrammiansolutionsofthisequation,respectively.ItisshownthatthesesolutionscanbeexpressedasnotonlyPfaffiansbutalsoWronskiansandGrammians.
简介:在现在的纸,包含三个任意的函数为的一个一般解决方案概括(2+1)维的KdV-mKdV方程,它被导出从概括(1+1)维的KdV-mKdV方程,首先借助于Wiess被介绍,小鼓,Carnevale(WTC)截断方法。然后有考虑的几条能量守恒定律的multisymplectic明确的表达被介绍为概括(2+1)维的KdV-mKdV方程基于桥的multisymplectic理论。随后,源于以便以Jacobi椭圆形的功能的合理功能模仿周期的波浪答案一般答案,一个半含蓄的multi-symplectic计划被构造那等价于Preissmann计划。从数字实验的结果,我们能断定multi-symplectic计划能精确地模仿周期的波浪答案概括(2+1)维的KdV-mKdV方程当时近似保存能量守恒定律。
简介:提出了一种新的基于数字信号处理器(DSP)TMS320LF2407A和专用驱动芯片ML4428的陀螺用无位置传感器无刷永磁直流电机(BLDCM)稳速控制系统。它采用芯片ML4428实现无刷直流电机速度控制系统中的反电势检测、换相和功率驱动,并使用数字信号处理器TMS320LF2407A作为控制处理器,实现了电机的起停控制、转速给定,转速检测。它还采用了锁相环技术和积分分离的PID控制算法,大大提高了系统的控制性能和可靠性。
简介:阴极材料李[CoxNiyMn1?x?y]为锂的O2第二等的电池被一条新线路作为一位先锋用分层的双氢氧化物(LDH)准备了。结果有-NaFeO2结构的分层的阶段在菱形的系统结晶,与有到0.47nm的夹层间距结束的空格组R-3m。X光检查光电子光谱学(XPS)被用来测量公司,Ni和Mn的氧化状态。在结构和李的电气化学的性质上改变Co/Ni/Mn比率的效果[CoxNiyMn1?x?y]O2被X光检查衍射和电气化学的测试调查了。产品表明了相当稳定的骑车行为,与为有Co/Ni/Mn=1/1/1的分层的材料的118mAh/g的一个可逆能力。
简介:ThecharacteristicsofsuspendedsedimentimagecanbereflectedbythecoefficientsofbiorthogonalwavelettransformofCDF(2,2).Basedonthepowerdistributionindifferentscales,anadaptivealgorithmisproposedinthispaper,wherebythecoefficientsareadjustednon-linearly.Theparticleinformationcanbewellretainedwhiletheuselessbackgroundisremoved.Inthisway,satisfactorybinaryimagecanbeobtainedforfurtheranalysisofthesedimentparticle.
简介:TiO2@ZrO2@Y2O3:有coremultishell结构的Eu3+合成粒子通过layer-by-layer(LBL)的联合被综合自己组装方法和一个solgel过程。获得的样品与扫描电子被描绘显微镜学(SEM),传播电子显微镜学(TEM),X光检查光电子光谱学(XPS),X光检查衍射(XRD),和荧光spectrophotometry。结果证明合成粒子有coremultishell结构,球形的形态学,和狭窄的尺寸分布。TiO2核心上的ZrO2层的存在能有效地阻止在TiO2核心和Y2O3壳之间的反应;为在在TiO2@ZrO2@Y2O3的TiO2核心和Y2O3壳之间的反应的温度:Eucoremultishell黄磷能被300提高
简介:TheinfluenceofNa2SO4ontheformationofZnOwhiskerswasinvestigatedinthispaper.ZnOwhiskerswithaspectratiosofupto50weresynthesizedbydissolvingε-Zn(OH)2precursorinNaOH/Na2SO4solutionatroomtemperature,followedbyagingoftheresultingsolutionat140℃for6h.Fouriertransforminfraredspectroscopy,Ramanspectroscopy,andX-rayphotoelectronspectroscopyanalysesrevealedthatSO42-ionswereprimarilyadsorbedonthe(100)planeoftheZnOwhiskersviaanouter-spherecomplexconfiguration(O-H…O),therebypromotingtheone-dimensionalgrowthofZnOwhiskersalongthec-axis.
简介:介绍了在中国科学院力学研究所JF12长实验时间激波风洞上开展的10°尖锥标模的天平测力实验研究结果.JF12激波风洞的实验时间为100~130ms,名义Mach数为7.0,喷管出口直径为2.5m,总焓为2.5MJ/kg,复现了35km高空的飞行条件.采用六分量应变天平,攻角分别为-5,0,5,10和14°,模型长度为1.5m,质量为50kg.实验结果表明,在100~130ms的实验时间里,应变天平的输出信号含有3~4个完整周期,可以通过对天平的输出信号进行平均直接获得气动力/矩测量结果,而不再需要进行加速度补偿,且气动力系数重复测量的不确定度小于2%.JF12激波风洞气动力系数的测量结果与传统高超声速风洞的结果符合得较好,表明在2.5MJ/kg的总焓下,真实气体效应对该模型气动力特性的影响不明显.
简介:TiO2nanoparticlesweresynthesizedbyahomogeneouscontrolledprecipitationmethodusingindustrialtitaniumsulfate(Ti(SO4)2).TheobtainedpowderswerecharacterizedbyX-raydiffraction(XRD),transmissionelectronmicroscope(TEM),Fouriertransforminfraredspectroscopy(FTIR)andICPplasmaspectrometer.EDTAwasusedascomplexingagenttoimprovethepurityandtheformationofTiO2nanoparticles.Experimentalresultsindicatedthatthehigh-purityTiO2nanoparticleswere20nminmeansizeandnearlymonodispersed.