简介:部分地,聪明切割的过程,缺陷由尺寸描绘了的结合的效果和在切开前后的内部压力上的2纸被使用破裂力学模型学习。有大尺寸的结合的缺陷是容易的引起缺点生长的严重偏差,这被发现,当切开时,导致薄层的一个非转移的区域。在结合的缺陷的内部压力是很小的一个实际聪明切割的过程,大界面的缺点总是在切开的过程支持缺点生长。同时,增加结合的缺陷的内部压力减少在切开前的缺点生长和它的偏差。stiffener限制的松驰的机制被建议澄清结合的缺陷的效果。而且,当结合的缺陷是在场的时,切开的过程的进步被分析。在切开以后,有大尺寸和高内部的压力的那些结合的缺陷在高温度的退火期间为薄电影的blistering是脆弱的。
简介:BasedupontheHellinger-Reissner(H-R)mixedvariationalprincipleforthree-dimensionalelasticbodies,themodifiedH-Rmixedvariationaltheoremformagnetoelectroelasticbodieswasestablished.Thestate-vectorequationofmagnetoelectroelasticplateswasderivedfromtheproposedtheorembyperformingthevariationaloperations.Tolayatheoreticalbasisofthesemi-analyticalsolutionappliedwiththemagnetoelectroelasticplates,thestate-vectorequationforthediscreteelementinplanewasproposedthroughtheuseoftheproposedprinciple.Finally,itispointedoutthatthemodifiedH-Rmixedvariationalprincipleforpureelastic,singlepiezoelectricorsinglepiezomagneticbodiesarethespecialcasesofthepresentvariationaltheorem.
简介:ThecharacteristicsofsuspendedsedimentimagecanbereflectedbythecoefficientsofbiorthogonalwavelettransformofCDF(2,2).Basedonthepowerdistributionindifferentscales,anadaptivealgorithmisproposedinthispaper,wherebythecoefficientsareadjustednon-linearly.Theparticleinformationcanbewellretainedwhiletheuselessbackgroundisremoved.Inthisway,satisfactorybinaryimagecanbeobtainedforfurtheranalysisofthesedimentparticle.
简介:Acompositebeamissymmetricifboththematerialpropertyandsupportaresymmetricwithrespecttothemiddlepoint.Inordertostudythefreevibrationperformanceofthesymmetriccompositebeamswithdifferentcomplexnonsmooth/discontinuousinterfaces,wedevelopanR(x)-orthonormaltheory,whereR(x)isanintegrableflexuralrigidityfunction.TheR(x)-orthonormalbasesinthelinearspaceofboundaryfunctionsareconstructed,ofwhichthesecond-orderderivativesoftheboundaryfunctionsareaskedtobeorthonormalwithrespecttotheweightfunctionR(x).WhenthevibrationmodesofthesymmetriccompositebeamareexpressedintermsoftheR(x)-orthonormalbaseswecanderiveaneigenvalueproblemendowedwithaspecialstructureofthecoefficientmatrixA:=[aij],aij=0ifi+jisodd.Basedonthespecialstructurewecanprovetwonewtheorems,whichindicatethatthecharacteristicequationofAcanbedecomposedintotheproductofthecharacteristicequationsoftwosub-matriceswithdimensionshalflower.Hence,wecansequentiallysolvethenaturalfrequenciesinclosed-formowingtothespecialtyofA.Weusethispowerfulnewtheorytoanalyzethefreevibrationperformanceandthevibrationmodesofsymmetriccompositebeamswiththreedifferentinterfaces.
简介:TiO2@ZrO2@Y2O3:有coremultishell结构的Eu3+合成粒子通过layer-by-layer(LBL)的联合被综合自己组装方法和一个solgel过程。获得的样品与扫描电子被描绘显微镜学(SEM),传播电子显微镜学(TEM),X光检查光电子光谱学(XPS),X光检查衍射(XRD),和荧光spectrophotometry。结果证明合成粒子有coremultishell结构,球形的形态学,和狭窄的尺寸分布。TiO2核心上的ZrO2层的存在能有效地阻止在TiO2核心和Y2O3壳之间的反应;为在在TiO2@ZrO2@Y2O3的TiO2核心和Y2O3壳之间的反应的温度:Eucoremultishell黄磷能被300提高
简介:TheinfluenceofNa2SO4ontheformationofZnOwhiskerswasinvestigatedinthispaper.ZnOwhiskerswithaspectratiosofupto50weresynthesizedbydissolvingε-Zn(OH)2precursorinNaOH/Na2SO4solutionatroomtemperature,followedbyagingoftheresultingsolutionat140℃for6h.Fouriertransforminfraredspectroscopy,Ramanspectroscopy,andX-rayphotoelectronspectroscopyanalysesrevealedthatSO42-ionswereprimarilyadsorbedonthe(100)planeoftheZnOwhiskersviaanouter-spherecomplexconfiguration(O-H…O),therebypromotingtheone-dimensionalgrowthofZnOwhiskersalongthec-axis.
简介:实验研究复杂波形结构引起平面界面变形和反射激波冲击下的R-M不稳定性的问题.在竖直激波管中生成稳定的N2/SF6平面界面,激波在圆柱绕射后,冲击平面界面,由此研究复杂激波引起的界面变形.平面激波在圆柱绕射后的流场,演化成具有初始入射波、三波点、弯曲反射波、Mach波和Mach反射产生的滑移线等复杂结构.研究复杂结构激波对界面的作用,对认识界面扰动的生成具有较大帮助.绕柱激波冲击后,平面界面仅在两对滑移线内部发生变形.绕柱激波冲击界面后,两对滑移线将界面分成"内界面"和"外界面",界面变形形态同滑移线和界面相交位置相关.反射激波二次冲击下,界面扰动的增长与Jacobs-Sheeley涡量模型较吻合.
简介:TiO2nanoparticlesweresynthesizedbyahomogeneouscontrolledprecipitationmethodusingindustrialtitaniumsulfate(Ti(SO4)2).TheobtainedpowderswerecharacterizedbyX-raydiffraction(XRD),transmissionelectronmicroscope(TEM),Fouriertransforminfraredspectroscopy(FTIR)andICPplasmaspectrometer.EDTAwasusedascomplexingagenttoimprovethepurityandtheformationofTiO2nanoparticles.Experimentalresultsindicatedthatthehigh-purityTiO2nanoparticleswere20nminmeansizeandnearlymonodispersed.
简介:PureAl2O3-2SiO2powderswerepreparedbysol-gelandcoprecipitationmethods,andtheiralkaliactivationreactivitieswerecompared.Thealkali-activationreactivityofthepowderpreparedbythesol-gelmethodwashigherthanthatofthepowderpreparedbythecoprecipitationmethod.Thepowderswereinvestigatedby27AIand29Simagic-anglespinningnuclearmagneticresonancespectroscopy(MASNMR)tounderstandtherelationshipbetweentheirstructureandalkali-activationreactivity.The27AlMASNMRdatashowedthatthefive-coordinateAIcontentofthepowderpreparedbythesol-gelmethodwashigherthanthatofthepowderpreparedbycoprecipitation.Thehighercontentoffive-coordinateAlcorrespondedtohigheralkali-activationreactivity.The29SiMASNMRdatashowedthatforthepowderpreparedbythesol-gelmethod,siliconwasreplacedbyaluminumatsecondarycoordinationsitesofthecentralSiatomsduringcalcination.However,forthepowderpreparedbysingle-batchcoprecipitation,themainchangewasfromalowdegreeofpolycondensationtoahighdegreeofpolycondensation.
简介:HomogeneousNi2+-dopedtitaniagelwassynthesizedbyasol-gelprocess,andthexerogelwasthenobtainedthroughaginganddrying,leadingtotheformationofNi/TiO2nanocompositeafterheattreatmentunderasuitablereducingatmosphere.TheresultingnanocompositewascharacterizedbyTGA-DSC,TEM,XRDandBETmethods.Theresultsshowthatthestructureandgrainsizeofthenanocompositescouldbemanipulatedbyalteringtheheat-treatmentconditions,andthatthenanocompositepossessesamesoporousstructurewithaporeradiusofca.28nmandaspecifictheanatase-rutilephasetransformation.
简介:DrivenbycuriosityaboutpossibleflightoptionsfortheChang’e-2spacecraftafteritremainsattheSun-EarthL2point,effectiveapproachesweredevelopedfordesigningpreliminaryfuel-optimalnear-Earthasteroidflybytrajectories.Theapproachesincludetheuseofmodifiedunstablemanifolds,gridsearchofthemanifolds’parameters,andatwo-impulsemaneuverfororbitalphasematchingandz-axisbiaschange,andaredemonstratedtobeeffectiveinasteroidtargetscreeningandtrajectoryoptimization.Asteroidflybysareexpectedtobewithinadistanceof2×107kmfromtheEarthowingtotheconstrainedEarth-spacecraftcommunicationrange.Inthiscase,thespacecraft’sorbitalmotionissignificantlyaffectedbythegravitiesofboththeSunandtheEarth,andtherefore,theconceptofthe"heliocentricoscillating-Keplerorbit"isproposed,becausetheclassicalorbitalelementsoftheflybytrajectoriesreferencedintheheliocentricinertialframeoscillatesignificantlywithrespecttotime.Theanalysisandresultspresentedinthisstudyshowthat,amongtheasteroidswhoseorbitsarethemostaccuratelypredicted,"Toutatis","2005NZ6",or"2010CL19"mightbeencounteredbyChang’e-2inlate2012or2013withtotalimpulseslessthan100m/s.
简介:Lithium-aluminum-cobalt-nickeloxideLiAlxCoyNi1xyO2particles,generallyusedascathodeoflithiumbattery,werepreparedbychemicalcoprecipitationfromanaqueoussolutionofLiOH,Al(NO3)3,Co(NO3)2andNi(NO3)2withNH4OH.XRD,SEMandFTIRwereusedtoexaminetheeffectofnickelcontentontheproduct.FTIRpatternsshowedthatincreaseinnickelcontentdecreasedtheabsorptionstrengthofthepeakofspinelstructureoftheproduct,attributedtotheoccupationbynickelinthealuminumsites.Particlesizeandelectricalpropertiesofthelithium-aluminum-cobalt-nickeloxide(abbreviatedasLACNO)particleswerealsodetermined.
简介:The(2+1)-dimensionalBKPequationintheHirotabilinearformisstudiedduringthiswork.WronskianandGrammiantechniquesareappliedtotheconstructionofWronskianandGrammiansolutionsofthisequation,respectively.ItisshownthatthesesolutionscanbeexpressedasnotonlyPfaffiansbutalsoWronskiansandGrammians.
简介:Thecoordinationpolymer,(Nd(H2O)5)2(2,6-AQDS)3·2H2Owhere2,6-AQDS=2,6-anthraquinonedisulfonate,hasbeensynthesisedviaahydrothermalroute.Structurally,itconsistsoflayersofmonomericNdpolyhedrawhicharelinkedby2,6-AQDSanionsformingapolymeric,three-dimensionalnetwork.EachNdatomisninecoordinate,bondingtofivewatermoleculesandtofouroxygenatomsfromfour2,6-AQDSanionswhichinturnpillarthelayersbybridgingtwoNdatomsinonelayer,andcoordinatingtoasingleNdintheother.
简介:NanocrystallineSnO2wassynthesizedbydirectmixingandgrindingofSnCI4-5H2OandNaOHatroomtemperature,followedbycalcinationatdifferenttemperaturesfordifferenttimesinair.ProductsampleswerecharacterizedbyX-raydiffractionandtransmissionelectronmicroscope,revealingthattheamorphousprecursorSnO2wastransformedtocrystalsat200℃for3h,andthattheaverageparticlesizeincreaseduponraisingthecalciningtemperatureorprolongingthecalciningtime.Themechanismofthephasetransformationoftheproductsisdiscussed.
简介:连贯的多角形的粒子的二维的分离元素模型(DEM)模拟被开发了估计点来源颤动的利益在楔形的hoppers导致流动。使用的particleparticle相互作用模型基于一个多接触原则。没有颤动,学习的第一部分在严肃下面调查了粒子分泌物决定批评的孔尺寸(Bc)就作为粒子形状的功能支撑流动。多角形形状的粒子比圆形的粒子需要一个更大的孔,这被显示出。当粒子顶点的数字增加,Bc减少,这也被显示出当粒子顶点的数字增加。圆形的粒子的增加以一种线性方式支持多角形的流动。学习的第二部分证明那颤动能提高流动,有效地减少Bc。模型表明了震荡器地点(高度)的重要性,与在提高的以前的连续统模型结果,和颤动振幅一致流动。
简介:Uniformlysizedα-Fe2O3hexagonalplateletsweresynthesizedbyahydrothermalprocessusingFe(OH)3suspensionandlargeamountofNaOH.ThereactionproductswerecharacterizedbyX-raydiffraction(XRD),scanningelectronmicroscopy(SEM),transmissionelectronmicroscopy(TEM),selectedareaelectrondiffraction(SAED),andavibratingsamplemagnetometer(VSM).Theresultsshowthatthehexagonalplateletsarefine,monodisperseandconsistingofsingle-crystals.Themagnetichysteresis(M-H)curveofthesamplesmeasuredatroomtemperatureindicatesthattheα-Fe2O3micro-plateletsexhibitferromagneticbehaviorswithrelativelylowcoercivity.