简介：本文应用静态工作点测量电路工作状态，应用动态波形测量法分析判断故障产生原因，对失真波形进行定量测量及分析原因。

简介：TheequilibriummolalitiesofIn3+inextractionreaction:In3+(aq)+3HOx(org)=In(Ox)3(org)+3H+(aq)weremeasuredationicstrengthsfrom0.13to2.54mol-kg-1intheaqueousphasecontainingNa2SO4asthesupportingelectrolyteandatconstantinitialmolalityofextractant,HOx,intheorganicphaseattemperaturesfrom278.15to308.15K,whereHOxandOxmean8-hydroxy-quinoliueanditsanion,respectively.ThestandardextractionconstantsK0atvarioustemperatureswereobtainedbytwomethodsproposedinourpreviouspaper.

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简介：Thispaperreportstwolanthanidecomplexesofformula（C9H7）Ln（C8H8）·（THF）2whereLnisProrNd,C9H7isindenyl,andC8H8iscyclooctatetraene（COT）.ThecomplexeswerepreparedbythereactionofLnCl3withK（C9H7）andK2（C8H8）inTHF.（C9H7）Pr（C8H8）·（THF）2crystallizesinTHFat-15℃inthemonoclinicspacegroupP21:withunitcelldimensionsa=8.446（0）,b=10.083（2）,c=13.407（3）,β=105.48（1）°,V=1100.43（35）3,Dc=1.52g/cm3andZ=2.ThefinalRvalueis0.033,Rwvalueis0.030,respectively.In（C9H7）Pr（C8H8）·（THF）2afive-memberedringcentroidofC9H7,theC8H8ringcentroidandthetwooxygenatomsfromthetwoTHFmoleculesformadistortedtetrahedralgeometryaroundthemetal.

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简介：一、填空题（每空1分，共25分）1．实验室里常用__________等仪器测物体的质量．若宇航员将一质量为2kg的矿石样本从月球带到地球上，它的质量是__________kg，物重是_______N．

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简介：ThedevelopmentoftheHalfWaveResonator(HWR010)isbasedontheChinaADSproject.TheHWR010operatesat162.5MHzandcanprovidemorethan0.78MVofacceleratingvoltagepercavityforprotonwithopt=0.10.ThegoaloftheRFpropertiesistogetalowerheatloadandahigheracceleratinggradient,whicharedeterminedbyahigherR/Q0andlowerpeaksurfacefields(Bpk/EaccandEpk/Eacc).InordertooptimizetheHWRgeometryparameters,CST-MWSisusedtoconducttheRFsimulation.TheoptimizedRFparametersareshowinTable1.

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简介：Thispaperreportsthattheetchingmorphologyofdislocationsin8°off-axis4H-SiCepilayerisobservedbyusingascanningelectronicmicroscope.Itisfoundthatdifferenttypesofdislocationscorrespondwithdifferentdensitiesandbasalplanedislcation(BPD)arrayandthreadingedgedislocation(TED)pileupgroupliealongsomecertaincrystaldirectionsintheepilayer.Itisconcludedthattheelasticenergyofthreadingscrewdislocations(TSDs)ishighestandTEDsislowestamongthesedislocations,sothedensityofTSDsislowerthanTEDs.TheBPDscanconverttoTEDsbutTSDscanonlypropagateintotheepilyerinspiteofthehigherelasticenergythanTEDs.ThereasonoftheformofBPDsarrayinepilayeristhatthebigstepalongthebasalplanecausedbyfacedefectsblockedtheupstreamatoms,andTEDspileupgroupisthatthedislocationsslideisblockedbydislocationgroupsinepilayer.

简介：Catalyticcombustionofpropane-airmixturewasinvestigated.Platinumcatalystsoveraflatstainlesssteelwithγ-aluminawashcoatwereemployed.Theemployedburnerhasthreecatalystssetparalleltothemixtureflow,spacedatanintervalof5,10and15mm.Bothexperimentandnumericalsimulationweremadeatinlettemperatureof553K,inletvelocityof3to7m/sandequivalenceratioof0.3to0.5.Inthenumericalsimulation,two-dimensional,steadystatemodelwasdevelopedtocalculatethetemperatureandspeciesconcentrationingas-phase.Inthismodel.chemicalreactiononthecatalystsurfaceandthatinthegasphasewereassumedtooccurinthree-steps.Thenumericalresultsshowgoodagreementwithexperimentalresults.Itwasfoundthatthepropertiesofthecatalyststronglyaffectthecatalystsurfacetemperature.Especially,thethermalconductivityofcatalysthasagreateffect,whiletheemissivityofcatalysthaslesseffect.

简介：ThefluorescenceemissionandX-raydiffractionofmagenesium8-hydroxyquinolinecomplex(Mgq2)havebeenmeasuredathighpressureupto14GPa.Ithasbeenfoundthatpressurecaninfluencetheemissiondramatically.Atrelativelowerpressure(lessthan2.5GPa)thefluorescenceofMgq2changesslightly,buttheemissiondropsquicklywithincreaseofthepressurewhenthepressuregetshigherthan2.5GPa.TheresultsofinsituenergydispersiveX-raydiffractionathighpressurewithsynchrotronradiationindicatethatthereisaphasetransitionatabout2.5-3GPaforMgq2crystal.2001ElsevierScienceB.V.Allrightsreserved.

简介：本文构造了一系列方程,由这些方程可以得到一年中任何一天、一天中任何一个时刻、从地球上任何纬度观察的太阳在天空中的位置。由这些方程出发,给出了太阳每年一次的8字形图的解释。这些方程还可以预测日出与日落时间。结合对8字形图的理解,本文证明了日出开始变早的时间为什么不是恰好在冬至时刻,而是在冬至以后的一段时间。在方程的构造中,模型假定地球环绕太阳运行的轨道是一个圆,且沿轨道匀速运动,利用日出的预测时间来评估由这个假设所引起的误差。

简介：Thedeuteronisalooselyboundstateoftwonucleons.Itisnaturaltoexpectotherboundstatescomposedoftwohadrons,thatis,hadronicmolecularstates[1].AftertheobservationbytheBelleCollaboration,theX(3872)wasrelatedtoalooselyboundstateofDˉDimmediatelyduetothefactthatitsmassisneartheDˉDthreshold.Recently,theBelleCollaborationannouncedtwochargedbottomonium-likestructuresZb(10610)andZb(10650)neartheBˉBandBˉBthresholds[2].TheanalysisoftheangulardistributionindicatedbothZb(10610)andZb(10650)favorIG(JP)=1+(1+).AstructureZc(3900)closetotheDˉDthresholdwasalsoobservedbytheBESIIIcollaborationinthedecayofY(4260),Y(4260)!+??J=[3].

简介：一荧光灯分核derivate，N-allyl-1-pyrenemethylammoniumhydrochloride(APA+)，被报导与葫芦形成稳定的hostguest建筑群[8]uril(CB[8])，并且这个性质能被利用到确定CB的纯净[8]经由排放滴定。而且，APA+和CB的1:1建筑群[8]能进一步绑甲基viologen(MV2+)，它是广泛地使用的除草剂的主要成分，提供一个好方法检测MV2+，特别在低集中。

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简介：8-羟基喹啉与许多金属元素（除碱金属外），在弱酸性或弱碱性溶液中能形成螯合物沉淀，这种沉淀分子量大，组成恒定。试样以硝酸和氢氟酸溶解，EDTA为掩蔽剂，在乙酸铵-乙酸（pH=6．5）的缓冲溶液中，8-羟基喹啉与钨生成黄色沉淀，灼烧称重无水WO3。分别对沉淀时pH值、陈化时间、沉淀剂的用量进行选择，研究出了一种快速、准确、经济的分析方法。分析准确度好、精密度高，完全能够满足生产分析要求。

简介：Lophenol,cholest-4α-methyl-7-en-3β-ol(1),obtainedfromDracaenacochinchinensis(Lour.)S.C.Chen,wasstructurallymodified.Itwasacetylatedtoprotect3β-hydroxylgroup,andthenoxidisedbyseleniumdioxideinaceticacidtogivecholest-4a-methyl-8-en-3β,Ta-dioldiacetate(3).Thiscompound3isunstableinchloroformsolutionorwhenheatedandeasilyconvertedtoadienecompound,cholest-4a-methyl-7,14-dien-3β-olacetate(4).Thestructuresof3and4wereelucidatedbymeansofIR,^1HNMR,^13CNMRandMS,andtheabsoluteconfigurationof3wasestablishedbyX-raycrystallography.Thepropertyof3wasalsodiscussedinthispaper.Both3and4arenewcompoundsandwerereportedforthefirsttime.