简介:AKerr-lens,mode-lockedYVO4∕Nd:YVO4lasercoupledwithanacousto-opticmodulator(AOM)Q-switchingnear1064nmwasemployedtopumpanintracavityKTiOPO4(KTP)opticalparametricoscillator.Asubnanosecondsignalwavenear1572nmwithlowrepetitionratewasrealized.AtanAOMrepetitionrateof8kHz,themaximumoutputpowerwas165mW.Thehighestaveragepulseenergy,theshortestduration,andthehighestpeakpowerofamode-lockingsignalpulsewereestimatedtobe~10.3μJ,~120ps,and~82kW,respectively.
简介:Li4Ti5O12(LTO)/carbonnanotubes(CNTs)compositematerialissynthesizedbasedonasolid-statemethodbysand-milling,spray-dryingandcalciningat8508CunderN2flow.TheLTO/CNTssampleswith1wt%and3wt%weightratioofCNTsadditionandthepristineLTOsampleareprepared.TherateperformanceandthethermalstabilityofthesesamplesareinvestigatedbasedonLiMn2O4(LMO)/LTOfull-cell.TheresultsshowthattheweightratioofCNTsadditionhasdistincteffectonLTOperformances.ThecompositematerialsofLTOcompositedCNTshavebetterperformanceathigh-rateduetotheintercalationenhancementbyconductivenetworkofCNTs.Atsecond,theoverchargingtemperatureresponseofthecell’ssurfacewith1wt%CNTsadditionisthelowest.Theparticlesizedistributionismeasuredandthemostuniformparticlesareobtainedwith1wt%CNTsaddition.ThistrendcouldexplainthatthemediumquantityofCNTsisoptimaltoimprovetheheatandmasstransferandpreventtheproblemsofcrystallitegrowinginterferenceandaggregationduringthecalcinationprocess.
简介:4-(Succinimido)-1-butanesulfonicacidasanefficientandreusableBronstedacidcatalyzedthesynthesisofpyrano[4,3-b]pyranderivativesundersolvent-freeconditions.Thecatalystcanbepreparedbymixingsuccinimideand1,4-butanesultonethatismoresimpleandsaferthanthepreparationofsuccinimidesulfonicacid.Thismethodhastheadvantagesofhighyield,cleanreaction,simplemethodologyandshortreactiontime.Thecatalystcouldberecycledwithoutsignificantlossofactivity.
简介:Isochronousmassspectrometry(IMS)instorageringsisapowerfultoolformassmeasurementsofexoticnuclewithveryshorthalf-livesdowntoseveraltensofmicroseconds,usingamulticomponentsecondarybeamseparatedin-ightwithoutcooling.However,theinevitablemomentumspreadofsecondaryionslimitstheprecisionofnuclearmassesdeterminedbyusingIMS.
简介:CO2methanationhasbeenahottopicbecauseofitsimportantapplicationinthespacecraftandpotentialutilizationofcarbondioxide.Nickelcatalystisactiveforthisreaction.However,itsactivitystillneedstobeimproved.Dielectricbarrierdischarge(DBD)plasma,initiatedatambientconditionandoperatedat~150°C,hasbeenemployedinthisworkfordecompositionofnickelprecursortoprepareNi/MgAl2O4.Theplasmadecompositionresultsinhighdispersion,uniquestructure,enhancedreducibilityofNiparticlesandpromotedcatalyst-supportinteraction.AnimprovedactivityofCO2methanationwithahigheryieldofmethanehasbeenachievedovertheplasmadecomposedcatalyst,comparedtothecatalystpreparedthermally.Forexample,themethaneyieldoftheplasmapreparedcatalystis71.8%at300°Cbutitis62.9%overthethermalpreparedcatalyst.ThecatalystcharacterizationconfirmedthatCO2methanationovertheDBDplasmapreparedcatalystfollowspathwayofCOmethanation.
简介:Alinear4-nodequadrilateralquasi-conformingplaneelementwithinternalparametersisproposed.Theelementpreservesadvantagesofthequasi-conformingtechnique,includinganexplicitstiffnessmatrix,whichcanbeappliedtononlinearproblems.Theweakpatchtestguaranteestheconvergenceoftheelement.ThenthelinearelementisextendedtothegeometricallynonlinearanalysisintheframeworkofTotalLagrangian(TL)formulation.Thenumericaltestsindicatethatthepresentelementisaccurateandinsensitivetomeshdistortion.
简介:TheinfluenceofNa2SO4ontheformationofZnOwhiskerswasinvestigatedinthispaper.ZnOwhiskerswithaspectratiosofupto50weresynthesizedbydissolvingε-Zn(OH)2precursorinNaOH/Na2SO4solutionatroomtemperature,followedbyagingoftheresultingsolutionat140℃for6h.Fouriertransforminfraredspectroscopy,Ramanspectroscopy,andX-rayphotoelectronspectroscopyanalysesrevealedthatSO42-ionswereprimarilyadsorbedonthe(100)planeoftheZnOwhiskersviaanouter-spherecomplexconfiguration(O-H…O),therebypromotingtheone-dimensionalgrowthofZnOwhiskersalongthec-axis.