One pot synthesis of a soluble polymer for zirconium carbide-中国期刊网

摘要 Anewpolymer,polyzirconoxanesal（PZS）,issynthesizedfromthereactionofzirconiumoxychlorideoctahydrate（ZrOCl2-8H2O）withacetylacetone（Hacac）andsalicylalcohol（SA）byone-potprotocol.Thepolymerissolubleincommonorganicsolvents,suchasethanol,methanol,acetone,tetrahydrofuranandchloroform,andexhibitsrheologywithviscosityof100-300mpasat25℃.Thesepropertiesaresuitableforusesinfabricationofceramicmatrixfibercomposites.Pyrolysisofthispolymerat1300℃inargonprovidesnanosizedZrCwithsphericalmorphologyandsizeof20-100nm.

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One pot synthesis of a soluble polymer for zirconium carbide

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One pot synthesis of a soluble polymer for zirconium carbide

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