AGaP/morinnanocompositematerialwasprepared,andthekeyfactorsaffectingtheluminescentpropertiesofthematerialwereinvestigated.IntenseluminescencewasobservedafterthecompositereactionbetweenGaPnanocrystalsandmorin.TheluminescenceoftheGaP/morincompositematerialisintensifiedremarkablywiththeratioofmorintoGaPnanocrystalsincreasing,butthepeakwavelengthremainsunchanged.WiththesizeofGaPparticlesdecreasing,theluminescentintensityofthecompositeincreasesandthepeakwavelengthblue-shifts.Thepossiblereasonforthisphenomenonwasdiscussed.