简介：Liquid-solid(L-S)masstransfercoefficients(Ks)werecharacterizedinagas-liquid-solid(G-L-S)three-phasecountercurrentmagneticallystabilizedbed(MSB)usingamorphousalloySRNA-4asthesolidphase.Effectsofsuperficialliquidvelocity,superficialgasvelocity,magneticfieldstrength,liquidviscosityandsurfacetensionwereinvestigated.ExperimentalresultsindicatedthattheexternalmagneticfieldincreasedKsinthree-phaseMSB,ascomparedtothoseinconventionalG-L-Sfluidizedbeds;thatKsincreasedwithmagneticfieldstrength,superficialgasandliquidvelocitiesanddecreasedwithliquidviscosityandsurfacetension;andthatKsshoweduniformaxialandradialdistributionsexceptforsmallincreasesclosetothewall.DimensionlesscorrelationswereestablishedtoestimateKsoftheG-L-ScountercurrentMSBusingSRNA-4catalyst,withanaverageerrorof3.6%.

简介：本文介绍航海－ⅢＧ型陀螺罗经用大功率三相正弦波脉宽调制中频静止电源，它由Ｅ－ＰＲＯＭ构成的可编程正弦波脉宽调制信号发生器、Ａ／Ｄ转换器组成的幅度调节器以及场效应管功率放大器等电路组成，输出频率、幅度、相位稳定的纯三相正弦波，具有效率高、负载能力强等优点，该电源还设置了多种故障检测、报警和多重过载保护电路，整机性能稳定，工作可靠。它不仅适用于航海型陀螺罗经的供电，对于其他功率较大的中频供电场合也是适宜的

简介：分布式联邦滤波器在多传感器信息融合领域得到广泛的重视，联邦滤波中的信息分配原则直接影响滤波器的精度和容错性，而常规的标量形式联邦滤波信息分配方法无法满足高动态环境下状态的动态变化特性。信息分配是设计和实现联邦滤波器的关键环节，基于系统误差协方差阵和可观测阵。文中考虑系统状态估计精度和系统的可观测性，提出了一种新的联邦滤波信息分配方案和算法。新的联邦滤波算法允许每一个系统状态变量具有不同的动态信息分配因子，从而改进了联邦滤波信息融合的精度。仿真结果表明，与传统联邦滤波算法比较，改进的信息融合算法精度能提高30％以上。

简介：Duetotheirsize-dependentpropertiesandflexibleprocessingchemistry(Alivisatos,1996),monodispersednanocrystalshaveattractedconsiderableattentionfortheirdistinguishedroleinfundamentalstudiesandtechnicalapplications.AlthoughmuchhasbeenreportedonfabricationofmonodispersedinorganicnanocrystalssuchasFe2O3,CdSe,PbSeandZrO2(Peng&Peng,2002;Zhuetal.,2002;Niederbergeretal.,2002;Pangetal.,2001),littlepublishedonthepreparationofBaSO4nanocrystalsandtheircrystalsizeandmorphologywhichaffecttheirperformanceinapplication.PolymeradditiveswithcomplexfunctionshavebeenusedastemplatestodirectorientednucleationandgrowthofBaSO4(Xiaoetal.,2001;Yuetal.,2002;Summersetal.,2002),asanewclassoffunctionalpolymers,theso-calleddouble-hydrophilicblockcopolymers,designedtocontrolthemorphologyofBaSO4(Colfenetal.,2002),includingtheirnanofiberssynthesizedinAOTmicroemulsion(Li&Mann,2000).ThoughsomuchresearchhasbeendevotedtocontrollingtheBaSO4morphologies,thepresentnotewillreportonthesynthesisofBaSO4nanocrystalswithsizecontrolling.

简介：

简介：

简介：

简介：Well-dispersedBaSO4nanoparticlesweresynthesizedinthepresenceofsodiumpolyacrylate（PAAS）byasimpleprecipitationmethod,withBaCl2and（NH4）2SO4asreactants.ThedifferentrolesperformedbyPAASinthesynthesisofBaSO4nanoparticleswereinvestigatedusingX-raydiffractometry,Fouriertransforminfraredspectroscopy,andtransmissionelectronmicroscopy.TheresultsindicatethattheassynthesizedBaSO4nanoparticlesweresphereswithanaveragediameterof30nmandthattheirsurfaceswereaffectedbythePAAS.Underatypicalprocedureemployed,PAASreactedwithBaCl2toyieldanintermediate,servingasacontrolreleasingagentandseparatingthenucleationandcrystalgrowthprocessesoftheBaSO4nuclei.DuringformationoftheBaSO4nanospheres,theintermediateslowlydissolvedandreleasedbariumandpolyacrylateions,inhibitingthegrowthandaggregationofnewlyformedBaSO4seedsandresultinginparticlesofnarrowdiameterdistributionandimproveddispersibility.Moreover,thesepolyacrylateionsfurthermodifiedthesurfacesoftheBaSO4nanoparticles.

简介：

简介：Fatiguepropertiesofage-hardenedAlalloy2017-T4underultrasonicloadingfrequency(20kHz)wereinvestigatedandcomparedwiththeresultsunderconventionalloadingofrotatingbending(50Hz).Thegrowthofacrackretardedatabout500μminsurfacelengthunderultrasonicloading,whileatabout20μmunderrotatingbending.Althoughstriationsbeingatypicalfracturemechanismwereobservedunderconventionalloading,mostoffracturesurfacewascoveredwithmanyfacetsunderultrasonicloading.Thesefacetswerealsoobservedunderrotatingbendinginnitrogengas.Thedifferenceingrowthmechanismdependingontheloadingfrequencyandtheretardationofacrackgrowthunderultrasonicloadingmaybecausedbytheenvironmentatthecracktipduetohighcrackgrowthrateunderultrasonicloading.

简介：TheinfluenceofNa2SO4ontheformationofZnOwhiskerswasinvestigatedinthispaper.ZnOwhiskerswithaspectratiosofupto50weresynthesizedbydissolvingε-Zn（OH）2precursorinNaOH/Na2SO4solutionatroomtemperature,followedbyagingoftheresultingsolutionat140℃for6h.Fouriertransforminfraredspectroscopy,Ramanspectroscopy,andX-rayphotoelectronspectroscopyanalysesrevealedthatSO42-ionswereprimarilyadsorbedonthe（100）planeoftheZnOwhiskersviaanouter-spherecomplexconfiguration（O-H…O）,therebypromotingtheone-dimensionalgrowthofZnOwhiskersalongthec-axis.

简介：有从30～80nm的尺寸的Fe3O4nanoparticles被湿milling铁粉末在一家行星的球工厂综合。阶段作文和同样综合的产品的形态学被X光检查衍射(XRD)测量，扫描电子显微镜学(SEM)和传播电子显微镜学(TEM)。NanosizedFe3O4粒子被湿milling准备金属性的铁粉末(?200网孔，99%)在与不锈钢装备的一家行星的球工厂，使用的小瓶与50:1并且以300rpm的旋转速度的ball-to-powder团比率在提取的水下面熨球。在这个方法的铁球的使用在Fe3O4formation起了一个关键作用。现在的技术简单，这个过程是容易的执行。

简介：

简介：Octahedron-likeBaMoO4microcrystalsweresynthesizedbytheco-precipitationmethodatroomtemperatureandprocessedinmicrowave-hydrothermalat413Kfordifferenttimes(from30minto5h).ThesemicrocrystalswereanalyzedbyX-raydiffraction(XRD),field-emissiongunscanningelectronmicroscopy(FEG-SEM)andtransmissionelectronmicroscopy(TEM).XRDpatternsshowedthatthismaterialpresentsatetragonalstructurewithoutthepresenceofdeleteriousphases.FEG-SEMandTEMmicrographsrevealedthattheBaMoO4microcrystalspresentanoctahedron-likemorphologywithagglomeratenatureandpoly-disperseparticlesizedistribution.Thesemicrographsalsoindicatedthatthemicrocrystalsgrowalongthe[001]direction.Theobservedcrystallographicplanesinthesestructuresweremodeledcomputationallyandacrystalgrowthmodelwasproposedinordertoexplainthemorphologicalchangesasafunctionofprocessingtime.

简介：TiO2nanoparticlesweresynthesizedbyahomogeneouscontrolledprecipitationmethodusingindustrialtitaniumsulfate(Ti(SO4)2).TheobtainedpowderswerecharacterizedbyX-raydiffraction(XRD),transmissionelectronmicroscope(TEM),Fouriertransforminfraredspectroscopy(FTIR)andICPplasmaspectrometer.EDTAwasusedascomplexingagenttoimprovethepurityandtheformationofTiO2nanoparticles.Experimentalresultsindicatedthatthehigh-purityTiO2nanoparticleswere20nminmeansizeandnearlymonodispersed.

简介：Thispaperestablishesanon-linearfiniteelementmodel(NFEM)ofL4-L5lumbarspinalsegmentwithaccuratethree-dimensionalsolidligamentsandintervertebraldisc.Forthepurpose,theintervertebraldiscandsurroundingligamentsaremodeledwithfour-nodalthree-dimensionaltetrahedralelementswithhyper-elasticmaterialproperties.Puremomentof10N·mwithoutpreloadisappliedtotheuppervertebralbodyundertheloadingconditionsoflateralbending,backwardextension,torsion,andforwardfle...

简介：