简介：ThethermodynamicphasestabilityareadiagramsofBCl3-NH3-SiCl4-H2-ArsystemwereplottedviaFactsagesoftwaretopredictthekineticexperimentalresults.Theeffectsofparameters（ie,partialpressureofreactants,depositiontemperatureandtotalpressure）onthedistributionregionsofsolidphaseproductswereanalyzedbasedonthediagrams.Theresultsshowthat：（a）Solidphaseproductsaremainlyaffectedbydepositiontemperature.TheareaofBN＋Si3N4phaseincreaseswiththetemperaturerisingfrom650to900℃,anddecreaseswiththetemperaturerisingfrom900to1200℃;（b）Whentemperatureandtotalpressureareconstants,BN＋Si3N4phaseexistsatahighpartialpressureofNH3;（c）Theeffectoftotalsystempressureiscorrelatedtodepositiontemperature.Thetemperaturerangingfrom700to900℃underlowtotalpressureistheoptimumconditionforthedeposition.（d）Appropriatekineticparameterscanbedeterminedbasedontheresultsofthermodynamiccalculation.Si–B–Ncoatingisobtainedvialowpressurechemicalvapordeposition.TheanalysisbyX-rayphotoelectronspectroscopyindicatesthatB–NandSi–Narethemainchemicalbondsofthecoating.

简介：一篇小说荧光灯为H2PO4-基于碳dots/Fe3+被设计并且制作合成。碳点被一个确定的一个壶综合热水的方法并且由传播电子显微镜，X光检查衍射计，紫外力的吸收分光计和荧光分光光度计描绘了。碳dots/Fe3+合成被碳点和FeCl3,的水的混合获得，它的荧光性质被荧光分光光度计描绘。碳点的荧光被水的Fe3+阳离子熄灭，导致碳dots/Fe3+的低荧光紧张合成。在另一方面，H2PO4-由化学反应减少了Fe3+的集中并且提高了碳dots/Fe3+的荧光合成。Stern-Volmer方程被介绍描述在合成的碳dots/Fe3+和H2PO4-,和好线性(R2=0.997)在H20.4-12公里的PO4-集中。

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简介：ZrC涂层被低压力在石墨底层上扔有Br的化学蒸汽免职(LPCVD)2-Zr-C3H6-H2-Ar系统。微观结构和ZrC涂层的生长行为上的免职时间的效果被调查。ZrC涂层在一个岛层模式成长了。涂层的形成被ZrC的成核统治在起始20分钟，和快速的成核产生了ZrC的有细密纹理的结构涂层。免职时间什么时候在30min上，涂层的生长被统治由晶体，给安排列的结构。精力散X光检查光谱学证明到锆的碳的臼齿的比率在在ZrC涂层，和X光检查的1:1附近显示出的光电子光谱学ZrC是在涂层的主要阶段，由大约2.5mol%伴随了ZrO2次要的阶段。

简介：制备了SO3H／SiO2自组装单层纳米膜材料，并用其在水中的质子化效应进行表征。用SO3H／SiO2作为吸附剂处理低浓度五氯酚（PCP）有机废水取得了良好的吸附效果。通过调节／不调节pH值对比吸附实验，推测PCP在SO3H／SiO2自组装单层表面的吸附机理为氢键吸附。

简介：Inordertorealizetheco-firingwithAg/Pdelectrodesinmultilayerdevices,Pb(Zn1/3Nb2/3)1-,-yZrxTiyO3(0.25＜x＜0.35,0.25＜y＜0.35)piezoelectricceramics(hereafterdesignatedPZN-PZT)modifiedbyLa2O3hasbeenpreparedbyconventionaltechniquewithsinteringtemperaturefrom1100℃to1140℃.X-raydiffractionpatternsdemonstratedthatpureperovskitephasewasobtained.Secondaryelectronimage(SEI)showedthatcrystallinegrainsinceramicswerewellgrown.d33ofmanufacturedsamplewasashighas560×10-12C/N.kpwasabout0.61andtgδabout30×10-3.TheexistenceofliquidphaseexaminedbyelectrondiffractioninPZN-PZTsampleisbeneficialtosinteringoftheceramic.

简介：用organo听Sn(OC4H9)4作为先锋，钠dodecylsulfonate(SDS)和SDS明胶(SDS-G)象模板复杂，二听二氧化物胶体的粒子被准备由一自己组装方法。两个SnO2产品分别地与SDS-G与SDS和SnO2-C粒子被标记SnO2-B粒子，它在制作相应于SnO2-B和SnO2-C传感器的SnO2煤气的传感器被使用。X光检查衍射(XRD)，扫描电子显微镜学(SEM)，传播电子显微镜学(TEM)和thermogravimetry和不同热分析(TG/DTA)被用于描述。试验性的结果证明SnO2-B胶体的粒子由mesoporous组成像片的粒子，当SnO2-C粒子主要由球形的粒子组成时。煤气的察觉到大小证明那个SnO2-B传感器执行察觉到反应到所有目标气体的最好，包括H2，C2H5OH和液体石油气体(LPG)。特别地，SnO2-B传感器的察觉到的反应在1000潩獮的集中在H2空气在32点被完成

简介：六角形的硼氮化物陶器(h-BN)基于B的nitridation，粉末被反应sintering获得方法。结果的产品的机械性质和微观结构上的sintering温度的效果被调查，反应机制被讨论。结果证明在B和N2之间的反应在从1000瀠潨潴畬業敮'諟Ｉⅹe数瑣潲捳灯?的温度有力地发生了堠爭祡瀠潨潴汥'虪箿e数瑣潲捳灯?堨卐?愠摮氠晩瑥浩?敭獡牵浥湥獴

简介：利用水热合成法制备了C-S-H凝胶，重点研究了不同的制备工艺、原材料与钙硅比对C-S-H凝胶结构的影响。经过详尽的X衍射（XRD）与核磁共振（NMR）分析表明，制备的样品都具备C-S-H凝胶的峰型特征；活性反应法相对于沉淀反应法制备的C-S-H凝胶层间距小、聚合度低；证实了C-S-H凝胶的层状结构，且层间距随钙硅比的增大而减小；Q^2／Q^1值与直链平均长度随钙硅比的增大而减小。

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简介：Sodiumparanitrophenolatedihydrate(NPNa·2H2O)isanexcellentsemiorganicnonlinearoptical(NLO)material,crystallizesbothinwaterandmethanolwithhighdegreeoftransparency.Goodopticalqualitysinglecrystalsofdimensionupto18mmx6mmx3mmareobtainedbyisothermalsolventevaporationtechnique.Thesolubilityofthecrystalindifferentsolventswasmeasuredgravimetrically.ThesinglecrystalsofNPNa·2H2Oshowvariationinphysicalpropertiesandgrowthrateindifferentsolvents.Methanolorethanolsolutionyieldscrystalsofbipyramidalshapewithclearmorphology.However,methanolgrowncrystalisexhibitingimprovedhardnessparametersandpossessesexcellentthermalstabilityascomparedtowatergrowncrystals.TheeffectsofsolventonhardnessparameteralongwiththermalandopticalpropertiesofNPNa·2H2Owasrevealedinthispaper.

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简介：TheagingbehaviorsofirradiatedtungstenbyhighenergySi3＋andH＋ionsaremainlyinvestigatedusinginternalfriction（IF）methodcombinedwithSEMtechnology.TheSEManalysisindicatesthatmoresevereirradiationdamageappearsinthesurfaceofsimultaneousdualSi3＋H＋irradiatedspecimenthanthatinthesequentialdualSi3＋H＋irradiatedspecimenorthesingleSi3＋irradiatedspecimensbecauseofthesynergisticeffectofSiandHirradiation.TheIFbackgroundoftheirradiatedsampleisaboutoneorderofmagnitudehigherthanthatoftheunirradiatedsampleowingtotheexistenceofhighdensityfreshdislocationsinducedbySi/Hirradiation,InthesequentialdualSi3＋andH＋irradiatedspecimen,thehydrogenSnoek-Ke-Koster（SKK）peakassociatedwiththemovementofdislocationsdragginghydrogenatomsisobservedanditsheightdecreaseswithagingtimeatroomtemperature.AsforthesimultaneousdualSi3＋H＋irradiatedspecimen,however,thereisnosuchhydrogenSKKpeak.Thereasoncanbeexplainedashydrogendiffusionandpinningeffectofdislocations.

简介：ThetransportpropertiesintheLa2/3(Ca1-xSrx)1/3MnO3(x=0,1/3,2/3)filmspreparedusingtheRFmagnetronsputteringmethodwereinvestigated.TheeffectoftheCa,Srdouble-dopingattheApositionintheLa2/3A1/3MnO3onthestructureofthetargetsandtransportofthefilmshasbeenstudied.Withtheincreaseofx,thestructuresofthetargetstransformfromtherhombohedralphasetothecubicphase;themetal-insulatorphasetransitiontemperature(Tp)ofthefilmsincreases;andthecorrespondingpeakresistivitydecreases.Allthephenomenacanbequalitativelyexplainedbythelatticeeffect.

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简介：Lowtemperaturecompositechromizingisaprocesscomposedofaplainion-carbonitridingorion-nitridingat550～580℃,followedbyalow-temperaturechromizinginasalt-bathof590℃.ThemicrostructureandpropertiesofthelowtemperaturecompositechromizedlayeronH13toolsteelwereinvestigatedusingmetallography,X-raydiffraction,microanalysis,hardnessandweartests.Itwasfoundthatthislowtemperatureprocesswasthermodynamicallyandkineticallypossible,andthecompositechromizedlayeronH13steel,withathicknessof3～6μm,consistedofthreesub-layers(bands),viz.theouterCr-richone,theintermediate(black)one,andtheinner,originalwhitelayer.Afterchromizing,theformerdiffusionlayerwasthickened.TheresultsofX-raydiffractionshowedthatthecompositechromizedlayercontainedsuchnitridesandcarbidesofchromiumasCrN,Cr2N,(Cr,Fe)23C6,and(Cr,Fe)7C3,aswellasplainα-(Fe,Cr).Ahighsurfacemicrohardnessof1450～1550HV0.025,whichismuchhigherthanthatobtainedbytheconventionalioncarbonitridingandionnitriding,wasobtained.Inaddition,anexcellentwearresistancewasgainedonthecompositechromizedlayer.

简介：CH3SiCl3(山)-H2-Ar系统被使用了原文如此与化学蒸汽免职(CVD)准备电影在这份报纸的方法。为三个方面原文如此拍摄，对生长率，表面粗糙，厚度和相对密度的一些重要影响由山一致性带了主要与运动始於西班牙的纸牌赌博carlo(KMC)被讨论了方法。模拟结果证明与不同免职温度为到山(H2/MTS)的H2的摩尔比率有某个规模。当山一致性增加时，生长率和三个方面的表面粗糙都增加关系，它表明近似线性。当增加三方面厚度的趋势显然是不同的时，三个方面的厚度也增加。尽管三个方面的相对密度都增加，增加的趋势与山一致性增加显示出小差别。

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