简介:基于镍的复合的层被阳极化在五分钱板上准备在一75?wt%H3PO4答案包含NH4F。这层然后被galvanostatic控告/解除(GCD)对待直到黑外部层被分开,留下象为supercapacitors的没有文件夹的电极材料的镍板上的一部电影。这部电影由Ni组成的微结构描述表演(哦)2和NiO,和没有氟化物在同样获得的电影被发现。电气化学的测试证明这个没有氟化物的电影电极展出954的一个高电容?F圆形的二色性(CD)系列和polyacrylamide胶化电气泳动(页)。当聚合物支架和金属建筑群作为催化活跃中心工作了,BSA服务了。当到BSA的转变金属离子建筑群的有约束力的比率是5:1时,结果证明BSA的结构仍然保持未改变。而且,清除superoxide一??
简介:Vanadiumnitridewassynthesizedbyone-stepmethodusingV2O5andcarbonblackasrawmaterialsinnitrogenatmosphere.ThephasesofdifferentreactionproductspreparedindifferentreactiontemperatureswereanalyzedbyX-raydiffraction(XRD),andthedynamicbehavioroftheprocessofsynthesizingvanadiumnitride(VN)byone-stepmethodwasstudiedwithnon-isothermalthermogravimetry.Themechanismfunctionandkineticparametersofreactionprocesswerecalculatedbythermalgravimetricanalyses(TGA),andthereactionrateequationwasestablished.TheXRDresultsshowthatforthesamplestestedwithminimalVNafterholdingfor4hat1273K,themainphaseofproductsisVNat1476K,whilesomevanadiumnitridestransformintovanadiumcarbidesagainover1573K.ItisfoundthatN2isbeneficialtostimulatereductionandproceedcarbonizationreaction,andthereductionandnitridationreactioncanoccursimultaneously.TheactivationenergyofpreparingVNbyone-stepmethodis104.005kJ·mol-1,andthefrequencyfactoris470.52at1280–1358K,and150.052kJ·mol-1and2.359104at1358–1426K,respectively.
简介:EffectofTwo-timesAnnealingonCharacteristicsofTiNiShapc-memoryAlloyZhangJinbo,SunXu,WangFushengandHeYongjian(张金波(孙序)(王福生)(何勇健)...
简介:MoS_2,MoSe_2andWSe_2thinflakeswerefabricatedbythestandardmicromechanicalcleavageprocedures.ThethicknessandtheopticalcontrastoftheatomicthindichalcogenideflakesonSiO_2/Sisubstratesweremeasuredbyatomicforcemicroscopy(AFM)andspectroscopicellipsometer.Arapidandnondestructivemethodbyusingreflectionspectrawasproposedtoidentifythelayernumberof2DlayeredtransitionmetaldichalcogenidesonSiO_2(275nm)/Sisubstrates.Thecontrastspectraof2DnanosheetswithdifferentlayernumbersareinagreementwiththeoreticalcalculationsbasedonFresnel'slaw,indicatingthatthismethodprovidesanunambiguousandnondestructivecontrastspectrafingerprintforidentifyingsingle-andfew-layeredtransitionmetaldichalcogenides.Theresultswillgreatlyhelpinfundamentalresearchandapplication.