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  • 简介:NineteenL-N-2-hydroxyethylaminoacidsandL-N,N-bis(2-hydroxyethyl)aminoacidswerepreparedfromthereactionofchlorohydrinwithL-alanine,L-valine,L-leucine,L-isoleucine,L-phenylalanine,L-serine,L-thrcunine,L-glutamicacid,L-asparticacidandglycine.L-N,N,N’,N’-tetra(2-hydroxyethyl)cystinewaspreparedbythereactionofL-cystinewithchlorohydrin.

  • 标签: hydroxyethyl PHENYLALANINE LEUCINE GLYCINE tetra solubility
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  • 简介:本文主要考察湖南境内湘语九个方言点的“V+X+NL)”结构类型和地理类型。湖南方言“V+X+N(1,)”的类型共有四种,除了普通话中常见的句型“在+N(1.)”、“V+到+N(1.)”外,还有“V+体貌助词州(L)”和“V+体貌助词+在+N(1.)”。

  • 标签: 湘语 V+X+N(L) 结构类型 地理类型
  • 简介:ByusingOH-terminatedpolyaryletherdendrimerandN-Fmoc-glycineasrawmaterials,thedendriticpolyarylether2-aminoacetate(G3-NH2)wassynthesizedviatwostepreactions.G3-NH2asamacroinitiatorforthering-openingpolymerizationofγ-benzylL-glutamateN-carboxyanhydridewasinvestigated.Itisfoundthattheresultingcopolymerspossessedrelativelyhighmolecularweightandnarrowmolecularweightdistribution(1.12

  • 标签: 开环聚合反应 γ-苯甲基L-谷氨酸酯N-羧基酐 多肽 枝晶
  • 简介:Inthispaperwewillshowthatifanapproximationprocess{Ln}n∈Nisshapepreservingrelativetotheconeofallk-timesdifferentiablefunctionswithnon-negativek-thderivativeon[0,1],andtheoperatorsLnareassumedtobeoffiniterankn,thentheorderofconvergenceofDkLnftoDkfcannotbebetterthann2evenforthefunctionsxk,xk+1,xk+2onanysubsetof[0,1]withpositivemeasure.Takingintoaccountthisfact,wewillbeabletofindsomeasymptoticestimatesoflinearrelativen-widthofsetsofdifferentiablefunctionsinthespaceLp[0,1],p∈N.

  • 标签: 渐近估计 N-宽度 线性相关 次可微函数 逼近过程 线性关系
  • 简介:ThecommutatorsofsingularintegraloperatorswithhomogeneouskernelΩ(x)/|x|^narestudied,whereΩishomogeneousofdegreezero,andhasmeanvaluezeroontheunitsphere.ItisprovedthatΩ∈L(logL)^(k+1)(S^(n-1))isasufficientconditionsuchthatthek-thordercommutatorisboundedonL^2(R^n).

  • 标签: 转接器 单一积分算子 有界平均振动 傅里叶变换
  • 简介:N-acetyl-D-methionine,NaAcandtheremainsofN-acetyl-L-methioninedramaticallyaffectthepurificationofL-methioninewhenpurifiedfromthemixtureofenzymaticallydeacylatedN-acetyl-DL-methionine,leadingtoalowyieldconventionally.Here,thispaperreportsasuccessfulseparationandpurificationofbothL-methionineandN-acetyl-D-methioninebyanHion-exchangecolumn.ThepH,L-Metconcentrationandtheratiobetweenthecontentofsodiumcationandtheion-exchangecapacitywereoptimizedtoobtainthemaximumyield.Experimentalresultsindicatethat,undertheoptimizedconditions,theyieldsofL-methionineandN-acetyl-D-methioninecanreachashighas85%and75%,respectively.

  • 标签: L-蛋氨酸 N-乙酰基-D-蛋氨酸 N-乙酰基-DL-蛋氨酸 分离 纯化 脱酰作用
  • 简介:在分析了直流电机驱动芯片L298N的性能、结构的基础上,结合SPCE061AEMUBOARD单片机(61板),介绍实现驱动直流电机的转正反一种简单方法.文中给出了控制原理图,还给出来了控制直流电机正反转驱动程序。实际测试表明,利用该方法设计的直流电机驱动系统具有硬件结构简单、软件编程容易。

  • 标签: 直流电机 单片机 L298N
  • 简介:让b=(b_1,···,b_m),b_i∈Λ_(β_i)(R~n),1≤i≤m,0<β_i<β,0<β<1,[b,T]f(x)=∫_(R~n)(K是aCalderon-Zygmund的b_1(x)-b_1(y))···(b_m(x)-b_m(y))K(x-y)f(y)dy,核。在这篇论文,我们显示出那[b,T]从L~p(R~n)toF_p~被围住(β,∞)(R~n),以及[b,从L~p(R~n)的I_α]到F_q~(β,∞)(R~n),在哪儿1/q=1/p-α/n

  • 标签: 多线性转换器 Calderon-Zygmund核心 LIPSCHITZ空间 TRIEBEL-LIZORKIN空间
  • 简介:ObjectivesToevaluateantihypertensiveefficiencyandsafetyofanewdomesticofL-&N-typeCa^2+antagonist-eilnidipinewithimidaprilasapositivecontrol.MethodsAfter2weeks'placebowashingout,22patientsweretreatedwitheilnidipine5mgdailyand27patientsweretreatedwithimidapril5mgdaily.4weekslater,ifpatient'ssittingdiastolicbloodpressureisover90mmHg,his/herdosagewasdoubledforanother4weeks,theothersmeasuringupremainedtheirdosageunchangedforanother4weeks.Bloodpressure,heartrate,bloodandurineroutineexamination,serumglucose,serumchemicalexaminationincludingtotalcholesterol,triglyceride,HDL,LDL,transaminase,creatineetcandsidereactionswererecordedbeforeandafterthetrial.Datawereanalyzedstatistically.ResultsAfter8weeks'treatment,bloodpressurewassignificantlydecreased(P<0.05)inbothgroups,andthetwomedicineshadsimilarantihypertensiveeffects.Furthermore,thereducingofheartratewasstatisticallysignificantcomparedwithbaseline(P<0.01)inthecilnidipinegroup,butnotintheimidaprilgroup.Thenegativechronotropiceffectofcilnidipinehadlittleeffectoncontinuingthetherapy.Therewerenochangesonbloodandurineroutineexaminationandserumlipid,serumglucose,creatine,transaminaseandetcinbothgroups.Theirsidereactionsweremildandwell-tolerated.ConclusionsCilnidipinehasacon-vincingantihypertensiveeffectsimilartothatofimi-dapril.Especiallycilnidipinemaybeadministeredtopatientswithrelativelymildtachycardia.

  • 标签: 钙拮抗剂 西尼地平 抗高血压药物 药物不良反应
  • 简介:TheauthorsdiscussproblemsofapproximationtofunctionsinL^2(R^n)andoperatorsfromL^2(R^n1)toL^2(R^n2)byRadial-BasisFunctions.TheresultsobtainedsolvetheparblemofcapabilityofRBFneuralnetworks,abasicprobleminneuralnetworks.

  • 标签: 径向基函数 中性网络 逼近函数 算子
  • 简介:为了研究射影平面网格图的L(2,1)—标号,通过归纳综合的方法,研究了当3≤m≤8,3≤n<6时,射影平面网格图Gm,nL(2,1)—标号问题,得到了以下结果:(1)G3,3的L(2,1)—标号数为8;(2)当3≤m≤8,3≤n<6时,Gm,nL(2,1)—标号数的上界为9。

  • 标签: L(2 1)-标号 L(2 1)-标号数 射影平面网格图
  • 简介:Arareearthcoordinationsystemwasfirstinvestigatedasanewtypeofcatalystforthering-openingpolymerizationofα-aminoacidN-carboxyanhydrides(NCAs).Theresultsforthepolymerizationofγ-stearyl-α,L-glutamate(SLG)NCAusingneodymiumacetylacetonate(Nd(acac)3)-orneodymiumtris(2-ethylhexylphosphonate)(Nd(P204)3)-triethylaluminum-waterascatalystswerecomparedwiththoseusingconventionalcatalysts.Itwasfoundthatthehelicalpoly(γ-stearyl-L-glutamate)withhighmolecularweightaswellasnarrowmolecularweightdistributioncanbeobtainedinthepresenceofNd(acac)3/AlEt3-1/2H2O.ThepolymerobtainedwascharacterizedbyIRandNMRspectroscopy.

  • 标签: Rare earth COORDINATION catalyst RING-OPENING POLYMERIZATION
  • 简介:TheFe-Ti-Nmateralloywaspreparedthroughthein-situreactionofnitrogengaswiththeFe-Timelt.ScanningelectronmicroscoperesultsshowthattheparticlesuniformlydistributedintheironmatrixwereTiN.ThedeliberatelypreparedFe-Ti-Nmasteralloywasemployedforthe409Lferriticstainlesssteelinanattempttorefinetheas-castsolidificationstructure.ItwasfoundthattheeffectivenessofFe-Ti-Nmasteralloyonrefiningoftheas-cast409Lferriticstainlesssteelwasaffectedbyadditionlevel,holdingtimeandmeltstemperature.Itwasfoundthattheaverageequiaxedgrainsizedecreasedfrom1503μmto303μm,theproportionofequiaxedgrainzoneincreasedfrom14%to100%withincreasingtheFe-Ti-Nmasteralloyadditionlevelto2.5%.Theproportionofequiaxedgraindecreasedfrom85%to4%asthesolidificationtemperatureincreasedfrom1803Kto1883K.Whentheholdingtimereachedto8min,thesolidificationstructuresof409Lferriticstainlesssteelshowextremepointsintheproportionofequiaxedgrain.Itisclearthatthegrainrefiningefficiencygraduallyfadeawaywiththeincreasingoftheholdingtimeattheverybeginning.However,whentheholdingtimecontinuestoincreaseandexceedstheextremepoint,thegrainrefiningefficiencyoftheFe-Ti-Nmasteralloyrecoveredtoacertaindegree.Theexperimentalresultsmentionedabovehavebeenanalyzedintermsofthermodynamics.Underappropriateconditions,theFe-Ti-Nmasteralloyusedforgrainrefinementofthesolidificationstructureof409Lferriticstainlesssteelmayhavegoodprospectsforindustrialapplications.

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