简介:利用金相显微镜(OM)、X射线衍射仪(XRD)和扫描电镜(SEM)及能谱分析(EDS)等测试方法研究Nb含量对铸造TiAl-xNb(x=1,3,5,7;原子分数,%)合金组织的影响。结果表明:Nb含量为1%时,TiAl-Nb合金铸锭组织主要为单相的γ组织;随Nb含量升高,合金组织主要为α2/γ层片组织;并在层片组织间存在2种偏析,分别是网状β相和γ相,合金的层片晶团平均尺寸逐渐增加,β相的体积分数逐渐升高;当合金中Nb的含量从1%增加到7%,层片晶团平均尺寸由89μm增加至190μm,β相的体积分数从1.9%增至12.9%;随合金中Nb含量增加,β相中Nb含量增加而Cr含量减少,γ相的偏析区域宽度变窄。
简介:以真空自耗电弧熔炼技术熔炼名义成分为Ti-47Al-2Nb-2Cr-0.4(W,Mo)(摩尔百分数)的TiAl合金铸锭,并以该熔炼铸锭进行无包套的近等温锻造实验,研究该TiAl合金铸锭的高温可锻性、显微组织及拉伸性能。结果表明:在无包套的近等温锻造工艺中,该熔炼铸锭显示出较好的高温可锻性,经涂覆玻璃粉浆保护,铸锭在经过60%锻造变形后其锻饼表面无明显裂纹。TiAl合金的铸造组织由细小、均匀的层片状晶团(α2+γ)和少量存在于片层团界的等轴γ晶粒构成;经近等温锻造后,锻饼组织则主要由平均晶粒尺寸为20μm的等轴γ晶粒和一些破碎的片层组织构成,在一些难变形区域,依然存在弯曲变形的片层组织。室温拉伸性能检测表明,由于晶粒细化效应,锻饼的平均抗拉强度由铸锭的433MPa提高到573MPa。
简介:采用等离子旋转电极雾化工艺制备名义成分为Ti-47Al-2Cr-2Nb-0.2W(原子分数,%)的预合金粉末,并经热等静压致密化得到TiAl基合金坯料。对热等静压坯体进行包套锻造,始锻温度为1150~1200℃,并控制应变速率为0.1~0.01s-1,研究包套锻造后TiAl基合金的高温力学性能。结果表明,包套锻造后组织得到了一定程度的细化和均匀化,从而使合金的高温力学性能得到提高,但由于显微组织中有少量微裂纹存在,导致包套锻造TiAl基合金仍呈现较低的伸长率。TiAl基合金在进行高温拉伸时,首先在试样内部形成微裂纹或微孔,随拉伸过程的进行微裂纹或微孔扩展、连通,最终使试样断裂。
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简介:Thenormallycenteredelectronbeamandnon-centeredelectronbeamweldingofTiAltoTC4wasinvestigatedinordertoanalyzetheelectronbeamweldabilitybetweenTiAl/TC4dissimilarmaterials.MacroscopiccoldcrackeasilyoccurrednearTiAlsubstrateinthejoints.Theoptimaltensilestrengthwasrelatedtotheweldingheatinput.Theweldstructureswerecomposedofbulkycolumnargrainsandequiaxedgrains.Theisolatedphasesconsistedoflargequantitiesofα2-Ti3Alphase,smallquantityofB2phase,γ-TiAlphaseandYAl2phase.InsufficientmeltingofthebasemetaloccurredintheweldwhenthebeampositionleanedtotheTC4side.Thetensilestrengthcouldbeimprovedwhenthedeflectionwaslimitedintheoptimumrange.Otherwise,non-fusionzonewaseasilygeneratedintheweld,whichledtothelowtensilestrength.
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简介:Ti-basedfillermetalsmadebytransientsolidificationandnormalcrystallizationwereselectedforthevacuumbrazingoftheTiAlalloyand42CrMounderdifferentprocessingparameters.Theresultsshowthatthetensilestrengthofthejointoftransientsolidifiedfillermetalishigherthanthatofnormalcrystallizedfillermetalunderthesameprocessingparameters.Bytheanalysisofscanningelectronmicroscope(SEM)andX-raydiffracting(XRD),itisfoundthatthehigherstrengthmaybecausedbythegeneratingofTiAl,TiNiandTiCuattheinterfaceofjointmadebytransientsolidifiedfillermetal.
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