简介:ThespinelLiMn2O4-x(SO4)xcompoundcathodematerialsweresynthesizedbysolid-statereactionofthecalculatedamountsofLiOH·H2O,MnO2andMnSO4.Theresultsoftheelectrochemicaltestdemonstratedthatthesematerialsexhbitedexcellentelectrochemicalproperties.Thehighestreversiblecapacityoftheseseriesofcathodematerialswas-120mAh/g,andafter50cycles,thisreversiblecapacitywasstillaround116mAh/gwithnearly100%reversibleefficiency,whichrevealedthatdopedsulfateioncouldimprovethestructuralstabilityofspinel.
简介:ThesynthesisofanewtypeofX-ray-sensitivecompound'di-(1-hydroxylundecyl)diselenide'anditsapplicationinthepreparationofanewtypeofliposomewithX-raysensitivitywasreported.Thisnewliposomewassynthesizedtoencapsulatedoxorubicinhydrochloride(Dox),withitsphysicalandchemicalproperties,stability,andradiationsensitivitydetermined.BasedonthepH-gradientmethod,liposomalDoxwaspreparedviaultrasonicemulsificationandthenpurifiedonaSephadexG50mini-column.UVspectrophotometryandliquidchromatographywereusedtodetecttheencapsulationefficiencyandradiationsensitivityoftheDox-loadedliposome.Theresultsshowthatthroughchangesinreleaserate,thisliposomeshowsarelativeradiosensitivity.Intermsofradiationsensitivity,thedrugleakrateoftheX-ray-sensitiveDox-loadedliposomeincreasedgraduallyandpeakedat65.4%undertheX-rayradiationofadoseof10Gyormorethan10Gy,whichissignificantlydifferentfromthatofordinaryliposomes.Meanwhile,X-ray-sensitiveDox-loadedliposomehasagooddispersionstability,withanaverageparticlesizeofapproximate120nm.TheefficiencyofthisliposomeencapsulatingDoxwas75.84%,slightlylowerthanthatofordinaryliposomes.TheX-ray-sensitiveDox-loadedliposomeexhibitedsuspensionstabilitywithin30dofstorageat4°C,withoutvisibleprecipitation.Di-(1-hydroxylundecyl)diselenideissafeandnoncytotoxicandcomparedwiththoseofsyntheticphospholipidsitssynthesisislowcostanddoesnotrequirecomplexconditions.
简介:Analgorithmofcontinuousstage-spaceMCMCmethodforsolvingalgebraequationf(x)=0isgiven.Itisavailableforthecasethatthesignoff(x)changesfrequentlyorthederivativef'(x)doesnotexistintheneighborhoodoftheroot,whiletheNewtonmethodishardtowork.Letnbethenumberofrandomvariablescreatedbycomputerinouralgorithm.Thenafterrn=O(n)transactionsfromtheinitialvalueXo,X^*canbegotsuchthat[f(x^*)|<e-^cm|f(xo)|bychoosingsuitablepositiveconstantc.Anillustrationisalsogivenwiththediscussionofconvergencebyadjustingtheparametersinthealgorithm.
简介:Anecessaryandsufficientconditionofregularityof(0,1,…,m-2,m)interpolationonthezerosof(1-x)Pn-1α,β(x)(α>-1,β≥-1)inamanageableformisestablished,wherePn-1α,β(x)standsforthe(n-1)thJacobipolynomial.Meanwhile,theexplicitrepresentationofthefundamentalpolynomialswhentheyexist,isgiven.
简介:SINGULARITYANDQUADRATUREREGULARITYOF(0,1,...,m-2,m)─INTERPOLATIONONTHEZEROSOF(1-x)Pn-1αβ(x)ShiYingguang(史应光)(ComputingCe...
简介:ThesplittingofpotentialenergylevelsforgroundstateX2ΠgofOx2(x=+1,1)underspin–orbitcoupling(SOC)hasbeencalculatedbyusingthespin–orbit(SO)multi-configurationquasi-degenerateperturbationtheory(SO-MCQDPT).TheirMurrell–Sorbie(M–S)potentialfunctionsaregained,andthenthespectroscopicconstantsforelectronicstates2Π1/2and2Π3/2arederivedfromtheM–Sfunction.TheverticalexcitationenergiesforOx2(x=+1,1)areν[O+12(2Π3/2→X2Π1/2)]=195.652cm1,andν[O12(2Π1/2→X2Π3/2)]=182.568cm1,respectively.Allthespectroscopicdataforelectronicstates2Π1/2and2Π3/2aregivenforthefirsttime.
简介:YBa2Cu3Ox(YBCO)thinfilmsgrownondifferentsubstrateswithand/orwithoutEu2CuO4(ECO)bufferlayerwereinvestigatedbyX-raywideanglediffraction,reflection,diffusescatteringandtopography.TheresultsshowthatfortheyttriastabilizedZrO2(YSZ)substrate,thepresenceofanECObufferlayerimprovesthecrystallinequalityoftheYBCOfilm,whileanegativeeffectisobservedfortheSrTiO3(STO)substrate.ThelateralcorrelationlengthforasamplegrownonaYSZsubstratewithECObufferLayerismuchgreaterthangrownonanSTOsubetrate.TheSTOsubstrateusedhasmosaicstructure.2001ElsevierScienceB.V.Allrightsreserved.
简介:作为X光检查,计算断层摄影术(CT)广泛地在诊断和放射疗法被用作,减少象一样低的放射剂量是重要的相当可完成。为这个目的,一个人可以使用基于的TV方法或小浪框架基于方法重建从设计的减少的数字的高质量的图象。由使用仅仅照亮region-of-interest(ROI)的内部断层摄影术计划,而且,一个人能节省更多的放射剂量。在这份报纸,柔韧的小浪框架规则化基于模型为全球重建和内部断层摄影术被建议。模型能帮助减少巨大的稀少的设计矩阵的失配引起的错误。一个三系统的分解计划被使用把重建的图象分解成三不同部分:动画片,人工制品和噪音。由丢弃估计的人工制品和噪音部分,因此,重建的图象能与更少的噪音和人工制品被获得。类似于基于的图象恢复建模的另外的框架,模型能被裂口Bregman算法高效地解决。数字模拟证明建议模型以锋利的边,吝啬的结构的类似(SSIM),contrast-to-noise比率,相对错误和关联的保藏超过FBP和SART+TV方法。为真实绵羊肺重建,当FBP和SART+TV方法需要超过200设计时,例如,建议方法能到达用仅仅100设计象0.75一样高的吝啬的结构的类似。另外,建议柔韧的方法为有与FBP和SART+TV方法相比的更好的性能的内部、外面的断层摄影术是适用的。