学科分类
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5 个结果
  • 简介:Theinfluenceofthehystereticbehaviourinreactivesputteringwithapurealuminiumtargetinthepresenceofargonandoxygenplasmaontransmittanceandsurfacefreeenergyofaluminiumoxidefilmswasinvestigatedbyplasmaopticalemissionspectroscopytechnology.Theevolutionsofaluminium,andaluminiumoxideemissionlinesasfunctionsofoxygenflowrateatconstantpowerandpressurewerestudied.Asteeptransitionfromthemetallicsputteringtothecompoundsputteringwasobserveduponincreasingtheoxygenflowratefrom0.0SCCMtoabove2.0SCCM.Thenanoptimaldepositionzonewasobtainedthroughanalyzingthehystereticcurvesofaluminiumandaluminiumoxideemissionlines.TheevolutionofcrystalstructuresofsampleswasdiscernedbyX-raydiffractionspectradata.EnergydispersiveX-rayspectroscopydataalsodemonstratetherelationshipbetweenthechemicalcompositionsofaluminiumoxidefilmsandthehystereticbehaviour.Thefilmdepositedbetween1.5SCCMand2.0SCCMoxygenflowratedisplaysanoptimalandstoichiometicatomicratioofOtoAlandmassratioofOtoAl.ThechangesinthetransmittanceofsampleswerediscoveredtodependontheoxygenflowratebyUV-VIStransmittancespectra,andthechangesinsurfacefreeenergywerestudiedbycontactanglemeasurement.

  • 标签: 铝氧化膜 磁控溅射 晶体结构 铝靶 等离子体发射 表面自由能
  • 简介:Indiumtinoxide(ITO)transparentconductingfilmwastreatedwithoxygenplasmaimmersionionimplantation(PIII).X-rayphotoelectronspectroscopy(XPS)wasemployedtocharacterizetheeffect.Theresultssuggestedthattheoxygencontentinthesurfacewasincreasedandmaintainedformorethan50hcomparedwithtraditionalplasma-treatedsamples.Meanwhile,theworkfunctionofITOestimatedbycomparingthepeakshiftintheXPSdiagramsuggestedacorrespondingincreasebymorethan1eV.

  • 标签: 等离子体浸没离子注入 氧化铟锡 功能增强 X射线光电子能谱 过氧 等离子体处理
  • 简介:Nanocrystallineoxidedispersionstrengthened(ODS)ferriticsteelpowderswithnominalcompositionofFe-14Cr-3W-0.3Ti-0.4Y2O3aresynthesizedusingsol-gelmethodandhy-drogenreduction.AtlowreductiontemperaturetheimpurityphaseofCrOisdetected.AthigherreductiontemperaturetheimpurityphaseisCr2O3whicheventuallydisappearswithincreasingreductiontime.ApureODSferriticsteelphaseisobtainedafterreducingthesol-gelresultantproductsat1200℃for3h.TheHRTEMandEDSmappingindicatethattheY2O3particleswithasizeofabout15nmarehomogenouslydispersedinthealloymatrix.ThebulkODSferriticsteelsamplespreparedfromsuchpowdersexhibitgoodmechanicalperformancewithanultimatetensilestressof960MPa.

  • 标签: 氧化物弥散强化 铁素体钢 还原合成 凝胶法 溶胶 表征