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简介：采用金相组织观察、力学性能测试和统计分析等手段,研究了成品退火工艺对Φ5mmTP2内螺纹铜管微观组织和力学性能影响规律。结果表明:Φ5mmTP2内螺纹铜管退火温度为470~480℃时,铜管组织细小、均匀,同时能获得较高塑性和较高强度;490~500℃时,铜管晶粒尺寸、力学性能波动大;510~520℃时,铜管组织易粗大。Φ5mmTP2内螺纹铜管在470℃退火时,晶粒尺寸随退火时间的规律变化为d=0.0008t3-0.062t^2+1.7t-1.3,保温21min时,铜管再结晶基本完成,保温时间为28~31min时,铜管组织状态和综合力学性能最佳。

简介：本文用循环伏安测温（ＣＶＴ）热电化学外推方法首次研究了Ｃｕ２Ｓ阳极过程动力学性质。实验的塔费尔斜率ｂ值与按迟缓放电机理所导出的Ｔａｆｅｌ斜率ｂ的理论计算值相符。

简介：通过对氯化钻溶液生产实践的论证，本文对生产氯化钴溶液萃取过程中影响其品质因素进行了分析和总结，提出了在现有工艺和技术条件下，生产氯化钻溶液在萃取过程中的最佳温度、pH值、皂化率及流比。

简介：Glasseswiththecompositionof65GeO212Ga2O3-10BaO-8Li2O-5La2O3(molarratio)dopedwith1.526wt.%,3.006wt.%,5.836wt.%,11.028wt.%,and15.678wt.%Tm2O3,respectively,werefabricatedbyconventionalmeltingmethod.AccordingtotheabsorptionspectraandtheJudd-Ofelttheory,theJ-Ostrengthparameters(Ω2,Ω4,Ω6)werecalculated,withwhichtheradiativetransitionprobabilities,branchingratiosandradiativelifetimeswereobtained.Theinfraredemissionspectra(with808nmLDexcitation)at～1.47and～1.8μmofvariousconcentrationsofTm3+-dopedglasseswerestudied.Theemissionintensityat～1.8μmreachedtothemaximumwhentheTm2O3-dopingconcentrationwasneartobe～3.006wt.%(1.0mol.%),andthendecreasedasdopingconcentrationincreasedfurther.Themechanismofthefluorescenceintensitychangewasexplainedwiththecross-relaxationeffectandtheconcentrationquenchingeffectofTm3+.Meanwhile,accordingtoMcCumbertheory,theabsorptionandemissioncross-sectionscorrespondingtothe3F4→3H6transitionsofTm3+at1.8μmwasobtained.ForTm3+-dopedgermanateglasses,themaximumemissioncross-sectionreachedavaluehigherthanthatre-portedforfluorozircoaluminateglasses.Itisexpectedtobeafavorablecandidatehostfor～2.0μmmid-inflatedlaserbecausetheglassshowsfavorableopticalspectra.

简介：Theaimofthisresearchistopulseco-depositnano-CeO2particlesintoNi-W-Balloycoatingsinordertoimprovethesurfaceproperties.Theinfluenceofpulsefrequencyanddutycircleondepositionrate,microhardnessandmicrostructures,andtheinfluenceofheattreatmenttemperatureonphasestructures,microhardnessandabrasivityofNi-W-B-CeO2compositecoatingswereinvestigated.Theresultsindicatedthatthepulseco-depositionofnickel,tungsten,boronandnano-CeO2particlefromthebathwhichnano-CeO2particlewassuspendedbyhighspeedmechanicalstirringledtotheNi-W-B-CeO2compositecoatings,possessingbettermicrohardnessandabrasionresistancewhenheat-treatedat400℃for1h.Themicrohardnessas-depositedwith636Hzandthedepositionratewith0.0281mm·h-1wasthehighestatpulsefrequencywith1000Hzandpulsedutycirclewith10%.Microstructuresanalysisdisplaysthatdecreasingpulsedutycycleleadstorefinementingrainstructuresandtheimprovementofmicrostructures.X-raydiffractionshowsthatthecompositecoatingas-depositedwasmainlyintheamorphousstateandpartiallycrystallized,butwhenheattreatedat400℃,thecrystallizationtrendwasstrengthenedfurther.

简介：通过运用工艺流程参数梳理,分析影响余热发电的制约原因,找出关键影响因素,并提出必要可行的措施,包括优化原料结构、强化烧结生产操作、完善现有工艺条件以及加强设备管理等.经过一系列有效措施的制定并实施后,余热发电量明显提升,在降低工序能耗的同时实现了稳定高效生产.

简介：ＥｌｅｃｔｒｏｎＭｉｃｒｏｓｃｏｐｉｃＩｎ－ｓｉｔｕＯｂｓｅｒｖａｔｉｏｎｆｏｒＰｒｅｐａｒａｔｉｏｎｏｆＵｌｔｒａｆｉｎｅＬａ２Ｏ３ＮａｎｏｐｈａｓｅＰｏｗｄｅｒＧａｏＹｕｚｕｎ（高愈尊），ＬｉＹｏｎｇｈｏｎｇ（李永洪），ＺｈａｎｇＴａｉｓｏｎｇ...

简介：OpticalabsorptionandemissionintensitiesofNd3+ioninKLu(WO4)2crystalwereinvestigated.BasedontheJudd-Offelttheory,wecalculatedthefollowingspectralparameters:phenomenologicalintensityparametersΩ2=5.567×10–20,Ω4=3.597×10–20,andΩ6=3.800×10–20cm2.Theradiativelifetimeoflevels4F3/2was182.58μs.Thefluorescencebranchingratioforthetransition4F3/2→4I11/2was46.98%.Inaddition,theradiativetransitionprobabilitiesAJ,J’,oscillatorstrengthsPJ,J’andthevaluesofinte...

简介：ＳｔｕｄｙｏｎＭｏｒｐｈｏｌｏｇｙｏｆＳｕｒｆａｃｅｏｆＬａｒｇｅＡｒｅａＹＢＣＯＴｈｉｎＦｉｌｍｓｏｎＺｒ（Ｙ）Ｏ２ＳｕｂｓｔｒａｔｅＷａｎｇＲｕｉｋｕｎ（王瑞坤），ＳｕｎＬｉｈｏｎｇ（孙丽虹），ＬｉｕＨｏｎｇｆｅｉ（刘鸿飞）ＷａｎｇＸｉａｏｐｉ?..

简介：采用高温固相法合成尖晶石LiMn2O4，并以化学沉积方式对其进行包覆氧化钴的表面处理。通过X射线衍射（XRD）、扫描电镜（SEM）等技术对表面处理前后的LiMn2O4进行表征，分析了表面处理后LiMn2O4物理特性的变化，并结合电化学性能测试，研究了表面处理及其工艺和条件对LiMn2O4电化学容量与循环性能的影响。结果表明，表面处理后LiMn2O4循环性能显著提高。随氧化物含量的增加，循环性能提高，容量降低。未经表面包覆的LiMn2O4首次充放电容量为108．13mAh／g，50次循环充放电后容量衰减26．3％。500℃加热处理的表面包覆0．5％、2％氧化钴的LiMn2O4首次循环放电容量各为118．38mAh／g、115mAh／g，经过50次充放电循环后，容量分别降低8％、7％。

简介：高度有效的Tb3+激活SrAl2O4黄磷被一个联合combustionsolid状态反应方法综合。SrAl2O4的先锋:Tb3+黄磷经由一个燃烧过程被准备，然后同样准备的粉末被加热在一减少在1250点的激活的碳周围??慥獲？

简介：DyPt2filmswerepreparedbyalternatedepositionthinDyandPtlayersonglasssubstratesbyDCmagnetocontrolledsputteringmethod.TheXRDdataindicatedthatforas-depositedDy/Ptfilms,andtheperiodiclayeredstructuresalongthicknessdirectionwereevidencedwithlowangleX-rayscattering.Withincreasingannealingtemperature,thecompoundsofDyPt,DyPt2andDyPt3wereformedsuccessivelyattemperaturerangingfrom300to400℃.ItwasfoundthatthecompositionreactionDyPt+DyPt3→2DyPt2tookplaceat500℃.Afterannealingat500℃for1h,thecompoundsDyPtandDyPt3transformedcompletelyintotheDyPt2compound.

简介：主要介绍了265m2烧结机自动化控制系统的结构及其主要控制功能,分析了故障诊断与报警、联锁的设计特点.该系统投运两年多来,运行平稳、质量可靠,取得了较好的成效.

简介：Forthegoalofsulfurrecovery,mostmethodsareaimedatthetailgaswithhigh-concentrationH2S,butfeweffectivemethodsareusedforlow-concentrationH2S.Inthiswork,Low-concentrationH2Scouldbepurifiedwellbyliquidphasecatalyticoxidation(LCO),andthesulfurresourcecouldalsoberecovered.TheabsorptionsolutionwaspreparedbyFeCl3andsulfosalicylicacid.Undertheexperimentalconditions,theconversionofH2StoScouldbemaintainedabove94%at60℃.InordertoenhancetheeconomicalefficiencyofLCOmethod,theabsorptionsolutionwasmodifiedbydopingCe,andaseriesofexperimentsweredesignedtoinvestigateitsperformance.TheresultsshowedthattheconversionofH2Shadnoobviousimprovement,butabove98%conversioncouldbegainedat60℃,andtheH2Sconversionratewasenhanced.TheoptimumadditionqualityofCe(NO3)3was0.08gto50mlFe3+solution.

简介：据行业网站报道，台湾烨联百分百转投资子公司“福建联德企业”的4条矿热炉（RKEF）镍铁生产线陆续运转，可于2月份全部投产，未来全产能可达到20万吨，可提供不锈钢厂炼钢使用。

简介：印尼国有镍金生产商PTAnekaTambang（Antam）的高级官员周二表示，公司计划建一年产能为2—2．7万吨镍的镍铁冶炼厂。

简介：TheeffectsofUVAphotoirradiatedCe(Ⅳ)dopedTiO2nanoparticle(CDTP)onratcoloncarcinomacellline(C26)growth,cellcycledistribution,andmorphologywerestudiedbyMTTassay,FlowCytometry,andfluorescentstaining.Theresultsindicatethatabout64.6%cellsarekilledafter24hby180μg·ml-1CDTPwhen8minexposedtoUVA,over90%deadfor30mingroup,relativeto18.7%,41.5%ofTiO2atthesameconditionrespectively.Hoe33258stainingofthefixedcellsrevealstypicalapoptoticstructures(apoptoticbodies),andcellsarearrestedinG0/G1phase.

简介：ThemorphologyandcorrosionbehaviorofNi/Al2O3compositecoatingspreparedusingdouble-pulsedelectrodepositingtechniqueafteroxidizedunder800℃NaCldepositinairenvironmentwereanalyzedbyscanningelectricalmicroscope(SEM),X-raydiffraction(XRD)andenergydispersivespectrum(EDS).TheresultsshowedthatthecorrosionofallcompositecoatingswasacceleratedunderNaCldeposits,andthecorrosionproductswereratherporouswithpooradherencetothematrix.Al2O3particlesinthecoatingscanrefinethegrainsizeandimprovethehightemperaturecorrosionresistanceofthecoatings.Withinthetestscope,themoreAl2O3particlesinthecoatings,thelowercorrosionratescouldbeobtained,andthecorrosionmechanismwasalsodiscussed.

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