简介：AGaP/morinnanocompositematerialwasprepared,andthekeyfactorsaffectingtheluminescentpropertiesofthematerialwereinvestigated.IntenseluminescencewasobservedafterthecompositereactionbetweenGaPnanocrystalsandmorin.TheluminescenceoftheGaP/morincompositematerialisintensifiedremarkablywiththeratioofmorintoGaPnanocrystalsincreasing,butthepeakwavelengthremainsunchanged.WiththesizeofGaPparticlesdecreasing,theluminescentintensityofthecompositeincreasesandthepeakwavelengthblue-shifts.Thepossiblereasonforthisphenomenonwasdiscussed.

简介：在之中无铅焊接材料，Sn-Ag-Cu合金有许多优点优异界面的性质和高度例如好弄湿的性质，爬抵抗。在这篇文章，组织和Sn-Ag-Cu材料的焊接性能被调查。二合金的表面形态学被实体镜的显微镜观察并且扫描电子显微镜(SEM)。化学宪法被X光检查精力散的光谱学(版本)检验。Sn-Ag-Cu的机械性质焊接Sn-Cu与那些相比系统地被评估焊接。结果证明Sn-Ag-Cu焊接基于不同焊接垫不同焊接性质。在接口的金属间化合的化合物(IMC)的厚度与老化时间增加。为镀金的垫，有很多IMC图，并且在焊接连接它能减少电的连接的可靠性。Sn-Ag-Cu焊接关节表演在传统的Sn-Cu上的一个优异机械性质焊接。酒窝减少和洞的数字增加因为Sn-Cu0.7合金和Sn-Ag3.0-Cu0.5合金的破裂表面有同类地分布式的许多小尺寸酒窝。

简介：Apilotwiredrawingmachineaswellaswireend-pointingrollerwasdeveloped.Usingthesemachines,awiredrawingtestforfourdifferentcoatingmaterialsandtwodifferentlubricantswasperformedasthereductionratioincreasedfrom10%to30%.Materialsusedforasubstrateinthisstudyareplaincarbonsteel(AISI1045)andultralowcarbonbainitesteel.Tocomputethefrictioncoefficientbetweenthecoatinglayerofwireandthesurfaceofdieforaspecificlubricant,aseriesoffiniteelementanalyseswerecarriedout.SEMobservationswerealsoconductedtoinvestigatethesurfacedefectsofwiredeformed.Resultsshowthatthebehaviorofdrawingforcevarieswiththelubricant-typeattheinitialstageofdrawing.Thepowder-typedlubricantwithalargeparticlecausestheretardationoffulllubricationontheentirecontactsurfaceandthelocaldelaminationofcoatinglayeronthewiresurface.Astheflowstressofasubstrateincreases,thedelaminationbecomessevere.

简介：Withtheassistanceofnonionicsurfactant(OP-10)andsurface-selectivesurfactant(CH3COOH),anataseTiO2waspreparedasananodematerialforlithiumionbatteries.Themorphology,thecrystalstructure,andtheelectrochemicalpropertiesofthepreparedanataseTiO2werecharacterizedbyscanningelectronmicroscopy(SEM),X-raydiffraction(XRD),electrochemicalimpedancespectroscopy(EIS),andgalvanostaticchargeanddischargetest.TheresultshowsthatthepreparedanataseTiO2hashighdischargecapacityandgoodcyclicstability.Themaximumdischargecapacityis313mAh·g-1,andthereisnosignificantcapacitydecayfromthesecondcycle.

简介：EmployingLi2CO3,NiO,Co3O4,andMnCO3powdersasstartingmaterials,Li[Ni1/3Co1/3Mn1/3]O2wassynthesizedbysolid-statereactionmethod.Variousgrindingaidswereappliedduringmillinginordertooptimizethesynthesisprocess.Aftersuccessiveheattreatmentsat650and950℃,thepreparedpowderswerecharacterizedbyX-raydiffraction(XRD)analysis,scanningelectronmicroscopy,andtransmissionelectronmicroscopy.Thepowderspreparedbyaddingsalt(NaCl)asgrindingaidexhibitaclearR3mlayerstructure.ThepowdersbyothergrindingaidslikeheptaneshowsomeimpuritypeaksintheXRDpattern.Theformerpowdersshowauniformparticlesizedistributionoflessthan1μmaveragesizewhilethelattershowsawidedistributionrangingfrom1to10μm.EnergydispersiveX-ray(EDX)analysissshowthattheratioofNi,Co,andMncontentinthepowderisapproximately1/3,1/3,and1/3,respecively.TheEDXdataindicatenoincorporationofsodiumorchlorineintothepowders.Charge-dischargetestsgaveaninitialdischargecapacityof160mAh·g-1forthepowderswithNaCladditionwhile70mAh·g-1forthepowderswithheptane.