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45 个结果
  • 简介:采用水热法合成了诺氟沙星金属配合物[Cu(C16H18N3FO3)2(C14H8O5)(H2O)3],并应用X-射线单晶衍射技术对其结构进行测定,确定了其几何构型,探讨了金属离子与药物分子的配位方式.采用琼脂扩散法对比4种常见细菌对药物的敏感性,结果表明合成的金属配合物具有一定的抑菌作用.

  • 标签: 诺氟沙星 金属配合物 合成 晶体结构 抑菌作用
  • 简介:InallthearticlesinActaMechanicaSolidaSinica,Volume31,Issues1-4thecopyrightisincorrectlydisplayedas"TheChineseSocietyofTheoreticalandAppliedMechanicsandTechnology"whereitshouldbe"TheChineseSocietyofTheoreticalandAppliedMechanics".

  • 标签: CORRECTION ACTA MECHANICA solida COPYRIGHT
  • 简介:Wehavedesignedandrealizedanathermal4-channelwavelength(de-)multiplexerinsiliconnitride(SIN).Minimizedthermalsensitivityisachievedinawidewavelengthrangebyusingwideandnarrowwaveguideswithlowanddifferentthermal-opticcoefficientsinthetwoarmsofMach-Zehnderinterferometers(MZIs).TheSiNcorelayerandSiO2claddinglayersaredepositedbyalow-temperatureplasma-enhancedchemicalvapordep-ositionprocess.ThefabricatedMZIfilterexhibitsathermalsensitivitywithin4-2.0pm/℃inawavelengthrangeof55nmtonear1300nm.Then,anathermal(de-)multiplexerbasedoncascadedMZIshasbeendemonstratedwithacrosstalk〈-22dBandathermalsensitivity〈4.8pm/℃forallfourchannels,reducedby77%comparedtoaconventionalSiN(de-)multiplexer.OwingtothepassiveoperationandcompatibilitywiththeCMOSback-endprocess,ourdeviceshavepotentialapplicationsin3Dintegrationofphotonicsandelectronics.

  • 标签: 氮化硅 通信技术 发展现状 材料学
  • 简介:对采用P栅增强技术的GaN功率晶体管进行了反应堆1MeV等效中子辐照效应实验。结果表明,在注量为1.5×10^15cm^-2的中子辐照后,器件的阈值电压没有发生明显变化;栅压较大时,辐照后的饱和漏电流变小,这与沟道电子迁移率降低和二维电子气2DEG的退化有关;当漏极电压小于200V时,器件的关态漏电流明显增加,表明中子辐照重掺杂P栅发生的载流子去除效应弱化了P栅在零栅压下对沟道电子的耗尽,但器件栅极反向泄漏电流在辐照后没有变化,说明其对中子辐照具有一定的免疫能力。

  • 标签: 氮化镓功率器件 增强型 栅注入晶体管 GAN 位移损伤效应
  • 简介:Inthiswork,SMAT(surfacemechanicalattritiontreatment)wasperformedonTi6Al4V.PlasmanitridingoftheSMATedsampleswasinvestigatedincomparisonwithcoarse-grainedsamples.Thesampleswerecharacterizedusingopticmicroscope,SEM,TEMandVickersmicrohardnesstester.TheresultsshowedthatasignificantlythickercompoundlayerwithhigherhardnesswasobtainedfortheSMATedsampleswhencomparedwithun-SMATedsamplesafternitriding.CorrosionresistanceofTi6Al4VinaRinger’ssolutionwasstudiedbyelectrochemicaltechniquesincludingopencircuitpotentialmeasurement,potentiodynamicpolarizationandEIS(electrochemicalimpedancespectroscopy).Overall,ourresultsidentifiedthebeneficialimpactsoftheduplexSMAT/nitridingtreatmentoncorrosionbehaviourofTi6Al4V.Weartestswerealsoperformedonaball-on-disctribometerwherethetreatedsampleswererubbedagainsta6mmdiameteraluminaballunderanormalloadof5NusingRinger’ssolutionaslubricantmedia.ThefrictioncoefficientoftheSMATedandnitridedsampleswasreducedcomparedtotheuntreatedsamples.WearratesdemonstratedthatSMATcombinedwithnitridingimprovedwearresistanceofTi6Al4Valloy.

  • 标签: Surface mechanical attrition treatment PLASMA NITRIDING
  • 简介:实验选取与抗炎免疫密切相关的磷酸二酯酶4为靶点,应用超滤液质联用技术和酶体外活性抑制实验筛选并鉴定了葛根中抑制磷酸二酯酶4活性成分.实验结果表明葛根提取物具有抑制磷酸二酯酶4的作用,IC50值为0.04g/L.葛根素抑制磷酸二酯酶4作用最强,其次为大豆苷和大豆苷元,IC50值分别为52.79,71.54和122.17μmol/L.超滤液质联用实验筛选结果与体外活性实验一致.3′-羟基葛根素和3′-甲氧基葛根素在2个实验中均没有抑制磷酸二酯酶4的作用.

  • 标签: 葛根 异黄酮 磷酸二酯酶4 超滤液质联用
  • 简介:ThenovelverticallystandingPtSe2filmontransparentquartzwaspreparedbyselenizationofplatinumfilmdepositedbythemagnetronsputteringmethod,andanNd:LuVO4passivelymode-lockedsolid-statelaserwasrealizedbyusingthefabricatedPtSe2filmasasaturableabsorber.TheX-raydiffractionpatternandRamanspectrumofthefilmindicateitsgoodcrystallinitywithalayeredstructure.ThethicknessofPtSe2filmismeasuredtobe24nmaccordingtothecross-sectionheightprofileoftheatomicforcemicroscopeimage.High-resolutiontransmissionelectronmicroscopyimagesclearlydemonstrateitsverticallystandingstructurewithaninterlayerdistanceof0.54nmalongthec-axisdirection.Themodulationdepth(AT)andsaturationfluence(Фs)ofPtSe2filmaremeasuredtobe12.6%and17.1μJ/cm2,respectively.Theobtainedmode-lockedlaserspectrumhasacentralwavelengthof1066.573nm,witha3dBbandwidthof0.106nm.Thetransformlimitedpulsewidthofthemode-lockedlaserwascalculatedtobe15.8ps.Amaximumaverageoutputpowerof180mWwithaworkingrepetitionrateof61.3MHzisobtained.Tothebestofourknowledge,thisisthefirstreportofthegenerationofultrafastmode-lockedlaserpulsesbyusinglayeredPtSe2asasaturableabsorber.

  • 标签: 磁控溅射法 通信技术 理论研究 发展现状
  • 简介:为了实现GPS信号缺失下的移动机器自主导航,解决传统粒子滤波中的粒子退化以及粒子贫乏引起的移动机器人定位和导航精度下降问题,提出了基于小生境理论的启发式蝙蝠优化粒子滤波的同时定位与地图构建算法。首先,在启发式蝙蝠优化算法的速度和位置更新过程中,引入惯性权重,加快了算法寻优精度,提高了收敛速度;然后,利用小生境理论进一步优化启发式蝙蝠算法,利用排挤机制和惩罚函数,有效地保证了种群的多样性,提高了算法的全局寻优能力;最后,将基于小生境理论的启发式蝙蝠优化算法用于传统粒子滤波采样中,使得粒子能够智能、快速地向高似然区域运动,同时提高了传统粒子滤波算法的全局寻优能力和寻优精度。实验结果表明:该算法显著提高了移动机器导航和定位的精度和实时性。

  • 标签: 同时定位与地图构建 粒子滤波 启发式算法 蝙蝠算法