简介:Amodelisproposedtocorrelatethecrackgrowthrateandstressratiocontainingveryhighcyclefatigueregime.Themodelisverifiedbytheexperimentaldatainliterature.Thenaformulaisderivedfortheeffectofmeanstressonfatiguestrength,anditisusedtoestimatethefatiguestrengthofabearingsteelinveryhighcyclefatigueregimeatdifferentstressratios.TheestimatedresultsarealsocomparedwiththosebyGoodmanformula.
简介:Veryhighcyclefatiguebehaviorsoftwobainite/martensitedual-phasesteelswereinvestigated.Oneofthesteelswascyclicrapidheattreatedanditsmicrostructureswererefined.Fatiguestrengthofthesteelis225MPahigherthanthatwithoutrefining.Observationoffracturesurfacesshowthatthefatiguecracksinitiateatbainitesfornon-refinedsteelandatnon-metallicinclusionsfortherefinedsteel.Thesizeofinclusionsismuchsmallerthanthatofbainiteswhichresultsintheimprovementoffatiguestrength.
简介:锁泉华的microfibrous网络由8m(dia)的3vol.%组成镍microfibers被利用了骗诱100200mdia的30vol.%。多孔的Al2O3。ZnO和CaO然后被早期的湿受精方法高度驱散到骗诱的Al2O3的毛孔表面上。由于表面区域,毛孔尺寸/粒子尺寸,热传导性,和空体积的唯一的联合,当在甲醇蒸气改过使用了时,产生microfibrous催化剂composites提供了催化的床反应和利用效率的重要改进。粗略地甲酸盐的260mL/min,包括>70%H2,<5%公司和踪迹CH4,与>97%甲醇变换,能在我们骗诱的新奇microfibrous的1cm3床卷被生产在470湩瑡潩?潰祬敭r合成的ZnO-CaO/Al2O3催化剂?鑈я鑈я8
简介:Anoveltwo-stagereductionprocessforsynthesisofultrafinenickelpowderwithahighpurityandlowdensityinafluidizedbedreactorhasbeendevelopedinthiswork.TherawultrafineNiOparticlesarefirstpre-reducedusinghydrogenatlowertemperatures(340-400℃),followedbyfurtherreductionathighertemperatures(500-600℃).Theself-agglomerationofNiparticlesformedduringlow-temperaturereductiondecreasesthesinteringactivityofthenewlyformedultrafineNiparticles,leadingtogoodfluidizationquality,evenforthesubsequenthigh-temperaturereductionprocess.TheagglomeratedNiparticleshaveahighNicontent(above99wt%),alowdensity(0.78g/cm~3)andauniformparticlesize(approximately100μm).Aconceptdesignforanoveltwo-stagefluidizedbedreactorprocessusedtoproducehigh-purityNipowderwasalsoproposed.Thisapproachmaybeextendedtothesynthesisofotherultrafine/nanosizedmetalsormetaloxidesthroughafluidizationmethod.
简介:Ultra-puremesoporoussilicamicrosphereswithgoodmonodispersityweresynthesizedintwosteps:nanometer-sizedsilicasolwasproducedbythesol-gelprocess,thenmicrometer-sizedsilicamicrospheresweresynthesizedbypolymerization-inducedcolloidaggregationofthesilicasol.Thetotalmetalcontentofthemicrosphereswasextremelylow,whicheliminatedthetailingofchromatographicpeaksbychelatingreagents.Theporestructureofthesilicamicrospherescouldbecontrolledbyalteringthesol-gelconditions.Thesilicamicrosphereparticlesizecouldbeadjustedbyusingdifferentpolymerizationinducedcolloidaggregationconditions.
简介:BSTOdielectricceramicwaspreparedfromSrTiO3andBaTiO3powderssynthesizedbyhydrothermalmethod,aswellasfromBa0.6Sr0.4TiO3powdersynthesizedbyconventionalsolid-statereaction.Theformercanbesinteredatarelativelylowtemperatureof1120℃.CharacterizationbySEMshowedthatthegrainshapesofbothceramicsarecubical,thoughthegrainsizeoftheformerismuchsmaller.Dielectricconstantsmeasuredat20℃wereshowntovarywithfrequencyintherangefrom1kHzto2MHzanddcbiasfield,andfurtherthatthedielectriclossoftheformertobelessthan2×10-3inthefrequencyrangeof20kHzto1MHz,muchsmallerthanthatofthelattersample.Fortheformer,temperaturedependenceofdielectricconstantismuchflatterandthereexistsanextendedphasetransitiondiffusioncoveringawidetemperaturerangeofCurietemperatureTc.Thesmallergrainsizeoftheformerdepressesthedcbiaselectricalfielddependenceofdielectricconstant.Thetunabilityis7%underabiasfieldof0.6kV/mmdc.
简介:Ammoniumsulfateresidueisaparticulatesolidandisproducedduringthemanufactureofammoniumsulfatefertilizer.Theresidueusedinthisstudycontainedalargeportionofcalciumcarbonate,fromwhichactivelime(CaO)wasrecoveredviathermaldecomposition.Weusedapurpose-builtdevicetodecomposetheresidueinasemi-suspensionstate.WefoundthatCaOhadthehighestactivitywhenresiduewasdecomposedat850-900℃.OurexperimentsindicatedthatammoniumsulfateresidueshouldbedecomposedinasuspensionstatetoproduceactiveCaO.Basedonourlaboratorytestfindings,anindustrial-scaleproductionlinewithahighsolid/gasratioinasuspensionstatewasdevised.TheoptimaloperatingconditionsforthedecompositionoftheammoniumsulfateresiduetoproducehighqualityCaOwerealsoinvestigated.WefoundthattheCaCO3decompositionratewashighandtheCaOproductwashighlyactive,averaging170sbythecitricacidmethod.MorphologymeasurementsshowedthattheCaOproducthadaporousstructureandalargespecificsurfaceensuringhighactivity.
简介:TiO2nanoparticlesweresynthesizedbyahomogeneouscontrolledprecipitationmethodusingindustrialtitaniumsulfate(Ti(SO4)2).TheobtainedpowderswerecharacterizedbyX-raydiffraction(XRD),transmissionelectronmicroscope(TEM),Fouriertransforminfraredspectroscopy(FTIR)andICPplasmaspectrometer.EDTAwasusedascomplexingagenttoimprovethepurityandtheformationofTiO2nanoparticles.Experimentalresultsindicatedthatthehigh-purityTiO2nanoparticleswere20nminmeansizeandnearlymonodispersed.
简介:Fastsolvinglarge-scalelinearequationsinthefiniteelementanalysisisaclassicalsubjectincomputationalmechanics.Itisakeytechniqueincomputeraidedengineering(CAE)andcomputeraidedmanufacturing(CAM).Thispaperpresentsahigh-efciencyimprovedsymmetricsuccessiveover-relaxation(ISSOR)preconditionedconjugategradient(PCG)method,whichmaintainstheconvergenceandinherentparallelismconsistentwiththeoriginalform.Ideally,thecomputationcanbereducednearlyby50%ascomparedwiththeoriginalalgorithm.Itissuitableforhigh-performancecomputingwithitsinherentbasichigh-efciencyoperations.Bycomparingwiththenumericalresults,itisshownthattheproposedmethodhasthebestperformance.